PMID- 23189658
OWN - NLM
STAT- MEDLINE
DCOM- 20130809
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 30
IP  - 7
DP  - 2012 Jul
TI  - [Rapid determination of pesticide multiresidues in vegetables and fruits by 
      accelerated solvent extraction coupled with online gel permeation 
      chromatography-gas chromatography-mass spectrometry].
PG  - 654-9
AB  - A novel method was developed for the rapid determination of 22 representative 
      pesticide residues in vegetables and fruits based on accelerated solvent 
      extraction (ASE) coupled with online gel permeation chromatography-gas 
      chromatography-mass spectrometry (GPC-GC-MS). The sample was extracted by 
      accelerated solvent extraction with dichloromethane-acetone (1:1, v/v) and 
      purified with a carbon/NH2 column, evaporated to dryness by nitrogen, then 
      dissolved in cyclohexane-acetone (7:3, v/v), and finally identified and 
      quantified by GPC-GC-MS system in selected ion monitoring (SIM) mode. The results 
      showed that the linearities of the 22 pesticides were good in their linear 
      ranges. The limits of detection (S/N = 3) were 0.3-1.8 microg/kg. The limits of 
      quantification (S/N = 10) ranged from 1-6 microg/kg. The recoveries for all at 
      three spiked levels in Chinese cabbages and apples ranged from 70.5% to 107.5% 
      with the relative standard deviations (RSDs) of 2.1%-8.7%. The proposed method is 
      accurate, sensitive and highly efficient in the extraction, and can be used for 
      the quick determination of the pesticide multiresidues in vegetables and fruits.
FAU - Ouyang, Yunfu
AU  - Ouyang Y
AD  - Changzhou Center for Disease Control and Prevention, Changzhou 213022, China. 
      ouyang1016@126.com
FAU - Tang, Hongbing
AU  - Tang H
FAU - Wu, Ying
AU  - Wu Y
FAU - Li, Guiying
AU  - Li G
LA  - chi
PT  - English Abstract
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Pesticide Residues)
RN  - 0 (Solvents)
SB  - IM
MH  - Chemical Fractionation
MH  - Chromatography, Gel/*methods
MH  - Food Contamination/analysis
MH  - Fruit/*chemistry
MH  - Gas Chromatography-Mass Spectrometry/*methods
MH  - Pesticide Residues/*analysis
MH  - Solvents
MH  - Vegetables/*chemistry
EDAT- 2012/11/30 06:00
MHDA- 2013/08/10 06:00
CRDT- 2012/11/30 06:00
PHST- 2012/11/30 06:00 [entrez]
PHST- 2012/11/30 06:00 [pubmed]
PHST- 2013/08/10 06:00 [medline]
AID - 10.3724/sp.j.1123.2012.03039 [doi]
PST - ppublish
SO  - Se Pu. 2012 Jul;30(7):654-9. doi: 10.3724/sp.j.1123.2012.03039.