PMID- 23277369 OWN - NLM STAT- MEDLINE DCOM- 20130625 LR - 20171116 IS - 1432-0800 (Electronic) IS - 0007-4861 (Linking) VI - 90 IP - 2 DP - 2013 Feb TI - Dissipation rates and final residues of kresoxim-methyl in strawberry and soil. PG - 264-7 LID - 10.1007/s00128-012-0952-9 [doi] AB - In order to study the dissipation rates and final residues of kresoxim-methyl in strawberry and soil, two independent filed trials were performed in Beijing China. The application rates are set at 195 g of active gradient per hectare. A simple analytical method has been developed for the determination of kresoxim-methyl in strawberry and soil. Kresoxim-methyl residues were extracted with acetonitrile from strawberry and soil samples which is determined by gas chromatography coupled with mass spectrometry detection (GC-MSD). The recoveries of kresoxim-methyl in strawberry and soil were observed from 78.9 % to 104.5 % at fortification levels of 0.01-0.5 mg/kg with relative standard deviations of 4.3 %-7.3 %. The reported limits of detection were 0.05 and 0.01 mg/kg for strawberry and soil, respectively. The results showed that kresoxim-methyl dissipation in strawberry could be described as first-order equation with the half-life time of 6.24 and 6.91 days. 14 days later, the dissipation rate is 84.9 % and 83.3 %, respectively. The final residues of kresoxim-methly in the strawberry were in the range of 2.7-4.8 mg/kg at pre-harvest intervals of 1, 3, 5, 7 days which is below the Japan maximum residue limits (MRLs) standards (5 mg/kg in strawberry). FAU - Jia, Chunhong AU - Jia C AD - Institute of Plant and Environment Protection, Beijing Academy of Agricultural and Forestry Sciences, Beijing, 100097, China. FAU - Zhu, Xiaodan AU - Zhu X FAU - Zhao, Ercheng AU - Zhao E FAU - He, Min AU - He M FAU - Yu, Pingzhong AU - Yu P FAU - Chen, Li AU - Chen L LA - eng PT - Journal Article PT - Research Support, Non-U.S. Gov't DEP - 20130101 PL - United States TA - Bull Environ Contam Toxicol JT - Bulletin of environmental contamination and toxicology JID - 0046021 RN - 0 (Fungicides, Industrial) RN - 0 (Methacrylates) RN - 0 (Phenylacetates) RN - 0 (Soil Pollutants) RN - 0 (Strobilurins) RN - 0LXZ062TTB (kresoxim-methyl) SB - IM MH - Fragaria/*metabolism MH - Fungicides, Industrial/*pharmacokinetics MH - Gas Chromatography-Mass Spectrometry MH - Half-Life MH - Limit of Detection MH - Methacrylates/pharmacokinetics MH - Phenylacetates/*pharmacokinetics MH - Reproducibility of Results MH - Soil Pollutants/*pharmacokinetics MH - Strobilurins EDAT- 2013/01/02 06:00 MHDA- 2013/06/26 06:00 CRDT- 2013/01/02 06:00 PHST- 2012/08/22 00:00 [received] PHST- 2012/12/21 00:00 [accepted] PHST- 2013/01/02 06:00 [entrez] PHST- 2013/01/02 06:00 [pubmed] PHST- 2013/06/26 06:00 [medline] AID - 10.1007/s00128-012-0952-9 [doi] PST - ppublish SO - Bull Environ Contam Toxicol. 2013 Feb;90(2):264-7. doi: 10.1007/s00128-012-0952-9. Epub 2013 Jan 1.