PMID- 23383486
OWN - NLM
STAT- MEDLINE
DCOM- 20140502
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 30
IP  - 10
DP  - 2012 Oct
TI  - [Determination of bisphenol diglycidyl ether residues in canned foodstuffs by 
      high performance liquid chromatography--tandem mass spectrometry].
PG  - 1002-7
AB  - An accurate quantitative determination and confirmative method for bisphenol 
      diglycidyl ether residues, bisphenol A diglycidyl ether (BADGE), bisphenol F 
      diglycidyl ether (BFDGE), bisphenol A (2,3-dihydroxypropyl) glycidyl ether (BADGE 
      H2O), bisphenol A bis (2,3-dihydroxypropyl) ether (BADGE x 2H2O), bisphenol A 
      (3-chloro-2-hydroxy propyl) (2,3-dihydroxypropyl) ether (BADGE x H2O x HCl), 
      bisphenol A (3-chloro-2-hydroxypropyl) glycidyl ether (BADGE x HCl), bisphenol A 
      bis(3-chloro-2-hydroxypropyl) ether (BADGE x 2HCl), bisphenol F bis (2, 
      3-dihydroxypropyl) ether (BFDGE x 2H2O), bisphenol F bis 
      (3-chloro-2-hydroxypropyl) ether (BFDGE x 2HCl) in canned foodstuffs by high 
      performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) has been 
      established. The sample was extracted with tert-butylmethyl ether and the extract 
      was cleaned-up and concentrated on a Waters Oasis HLB column. The target 
      compounds were analyzed by HPLC-MS/MS on a C18 column by the gradient elution 
      with methanol and 5 mmol/L ammonium acetate containing 0.1% formic acid in a 
      multiple reaction monitoring (MRM) scan mode. External matrix standard solutions 
      were used for the quantitative determination and the calibration curves showed 
      good linearity in the concentration range of 10.0 -2 000.0 microg/L for the nine 
      target compounds. The limits of quantification of the nine compounds were 10.0 
      microg/kg (S/N > or = 10). The average recoveries of the nine compounds ranged 
      from 79.6% to 100.9% at the spiked levels of 10.0, 100.0, 1 000.0 microg/kg with 
      the relative standard deviations (RSDs) of 6.3%-12.1%. The method is sensitive, 
      accurate, and suitable for the rapid determination of bisphenol diglycidyl ether 
      residues in canned foodstuffs.
FAU - Zhao, Xiaoya
AU  - Zhao X
AD  - Hubei Entry-Exit Inspection and Quarantine Bureau, Wuhan 430050, China. 
      zhaoxy@hbciq.gov.cn
FAU - Fu, Xiaofang
AU  - Fu X
FAU - Wang, Peng
AU  - Wang P
FAU - Li, Jing
AU  - Li J
FAU - Hu, Xiaozhong
AU  - Hu X
LA  - chi
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Benzhydryl Compounds)
RN  - 0 (Epoxy Compounds)
RN  - V3625OQU1K (bisphenol F diglycidyl ether)
SB  - IM
MH  - Animals
MH  - Benzhydryl Compounds/*analysis
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Epoxy Compounds/*analysis
MH  - Food Contamination/*analysis
MH  - Food, Preserved/*analysis
MH  - Meat/analysis
MH  - Tandem Mass Spectrometry/*methods
EDAT- 2013/02/07 06:00
MHDA- 2014/05/03 06:00
CRDT- 2013/02/07 06:00
PHST- 2013/02/07 06:00 [entrez]
PHST- 2013/02/07 06:00 [pubmed]
PHST- 2014/05/03 06:00 [medline]
AID - 10.3724/sp.j.1123.2012.08024 [doi]
PST - ppublish
SO  - Se Pu. 2012 Oct;30(10):1002-7. doi: 10.3724/sp.j.1123.2012.08024.