PMID- 23583948 OWN - NLM STAT- MEDLINE DCOM- 20131231 LR - 20191210 IS - 1873-3336 (Electronic) IS - 0304-3894 (Linking) VI - 254-255 DP - 2013 Jun 15 TI - Wipe sampling of amphetamine-type stimulants and recreational drugs on selected household surfaces with analysis by ultra-performance liquid chromatography quadrupole time-of-flight mass spectrometry. PG - 46-56 LID - S0304-3894(13)00188-X [pii] LID - 10.1016/j.jhazmat.2013.03.012 [doi] AB - Sorption characteristics of eight drugs related to recreational and clandestine activity-amphetamine, cocaine, heroin, N-formyl amphetamine, N-formyl methamphetamine, methamphetamine, 3, 4-methylenedioxymethamphetamine (MDMA), and pseudoephedrine-were evaluated on selected kitchen countertop surfaces. Methanol-dampened Whatman 40 filter paper wipes were used to collect samples from eleven surfaces including alkyd resin, ceramic tiles, glass, granite, laminate, limestone, marble, quartz compac, quartz real, soap stone, and stainless steel. The filter paper wipes were analyzed by a rapid three-minute UPLC-QTOF method, following ammonium acetate buffer (pH 5.8-6.2) extraction. The average percentage recoveries after 15 h of exposure to the surface materials tested, was found to be highest for cocaine and MDMA and lowest for amphetamine and methamphetamine. Among the eleven countertop surfaces, overall recoveries for marble were observed to be the least, whereas soapstone, quartz compac and stainless steel were among the highest. Scanning electron microscopic images of the surfaces provided a unique view of surface irregularities that potentially influenced drug recovery. Aging, migration, solvent composition, and volatility were examined. The variation in recovery of drugs was attributed to four key factors: compound volatility, surface composition, surface-compound interaction, and solvent composition. CI - Copyright (c) 2013 Elsevier B.V. All rights reserved. FAU - Madireddy, Sri Bharat AU - Madireddy SB AD - Department of Chemistry, 1 William L Jones Drive, Tennessee Technological University, Cookeville, TN 38505, United States. FAU - Bodeddula, Vanaja Reddy AU - Bodeddula VR AD - Department of Chemistry, 1 William L Jones Drive, Tennessee Technological University, Cookeville, TN 38505, United States. FAU - Mansani, Sravan Kumar AU - Mansani SK AD - Department of Chemistry, 1 William L Jones Drive, Tennessee Technological University, Cookeville, TN 38505, United States. FAU - Wells, Martha J M AU - Wells MJM AD - Department of Chemistry, 1 William L Jones Drive, Tennessee Technological University, Cookeville, TN 38505, United States. FAU - Boles, Jeffrey O AU - Boles JO AD - Department of Chemistry, 1 William L Jones Drive, Tennessee Technological University, Cookeville, TN 38505, United States. Electronic address: jboles@tntech.edu. LA - eng PT - Journal Article PT - Research Support, U.S. Gov't, Non-P.H.S. DEP - 20130315 PL - Netherlands TA - J Hazard Mater JT - Journal of hazardous materials JID - 9422688 RN - 0 (Amphetamines) RN - 0 (Central Nervous System Stimulants) RN - 0 (Illicit Drugs) RN - 7CUC9DDI9F (Pseudoephedrine) RN - I5Y540LHVR (Cocaine) SB - IM MH - Adsorption MH - Amphetamines/*analysis MH - Central Nervous System Stimulants/*analysis MH - Chromatography, Liquid MH - Cocaine/analysis MH - Housing MH - Illicit Drugs/*analysis MH - Mass Spectrometry/methods MH - Pseudoephedrine/analysis EDAT- 2013/04/16 06:00 MHDA- 2014/01/01 06:00 CRDT- 2013/04/16 06:00 PHST- 2012/10/24 00:00 [received] PHST- 2013/02/09 00:00 [revised] PHST- 2013/03/06 00:00 [accepted] PHST- 2013/04/16 06:00 [entrez] PHST- 2013/04/16 06:00 [pubmed] PHST- 2014/01/01 06:00 [medline] AID - S0304-3894(13)00188-X [pii] AID - 10.1016/j.jhazmat.2013.03.012 [doi] PST - ppublish SO - J Hazard Mater. 2013 Jun 15;254-255:46-56. doi: 10.1016/j.jhazmat.2013.03.012. Epub 2013 Mar 15.