PMID- 23593887
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20140728
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 30
IP  - 12
DP  - 2012 Dec
TI  - [Determination of six anthraquinone compounds in soil by parallel type dual 
      gradient high performance liquid chromatography].
PG  - 1282-6
AB  - A high performance liquid chromatography (HPLC) was established for the 
      determination of six anthraquinone compounds, 1,8-dinitroanthraquinone, 
      1,5-dinitroanthraquinone, 1-aminoanthraquinone, anthraquinone, naphthalene, 
      1,4,5,8-tetrachlorodibenzo anthraquinone, in polluted soil of residential 
      construction. In this method, by using an Ultimate dual gradient liquid 
      chromatograph (DGLC), designing a set of parallel dual system and accepting two 
      same Dikma Diamonsil C18 columns (150 mm x 4.6 mm, 5 microm) to cross-analysis, 
      41.46% of the analysis time can be saved. By using assisted ultrasonication to 
      the extraction of the six substances in the samples with 50 mL 
      N,N-dimethyl-formamide/1,4-dioxane/methanol (5/20/25, v/ v/v), the average 
      recoveries of the six analytes spiked in nine blank soil samples were 82.7% - 
      101% with the relative standard deviations (RSDs) of 1.8% - 3.2% and the limits 
      of detection were 0.007 - 0.054 mg/kg, which can reach the limited requirement of 
      the local standard in Beijing of DB11/T811-2011. With the advantages of 
      accessibility, high sensitivity and good reproducibility, this method can be used 
      in the determination of anthraquinone compounds in soil.
FAU - Ma, Hao
AU  - Ma H
AD  - Analysis and Research Center, East China University of Science and Technology, 
      Shanghai 200237, China.
FAU - He, Wei
AU  - He W
FAU - Yang, Liu
AU  - Yang L
FAU - Yin, Xuemei
AU  - Yin X
FAU - Wang, Wenjia
AU  - Wang W
FAU - Shi, Chaoou
AU  - Shi C
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2013/04/19 06:00
MHDA- 2013/04/19 06:01
CRDT- 2013/04/19 06:00
PHST- 2013/04/19 06:00 [entrez]
PHST- 2013/04/19 06:00 [pubmed]
PHST- 2013/04/19 06:01 [medline]
AID - 10.3724/sp.j.1123.2012.07037 [doi]
PST - ppublish
SO  - Se Pu. 2012 Dec;30(12):1282-6. doi: 10.3724/sp.j.1123.2012.07037.