PMID- 23768653
OWN - NLM
STAT- MEDLINE
DCOM- 20140121
LR  - 20171116
IS  - 1873-3778 (Electronic)
IS  - 0021-9673 (Linking)
VI  - 1300
DP  - 2013 Jul 26
TI  - Simultaneous determination of cyflumetofen and its main metabolite residues in 
      samples of plant and animal origin using multi-walled carbon nanotubes in 
      dispersive solid-phase extraction and ultrahigh performance liquid 
      chromatography-tandem mass spectrometry.
PG  - 95-103
LID - S0021-9673(13)00830-3 [pii]
LID - 10.1016/j.chroma.2013.05.052 [doi]
AB  - A rapid and effective method for the simultaneous determination of cyflumetofen 
      and its main metabolite residues in samples of plant and animal origin (tomato, 
      apple, eggplant, soybean, green tea, fish, and pork liver) was developed using 
      ultrahigh performance liquid chromatography-tandem mass spectrometry 
      (UPLC-MS/MS). Samples were extracted with acetonitrile and cleaned-up with 
      multi-walled carbon nanotubes (MWCNTs). The determination of the presence of 
      target compounds was achieved in less than 4.0min using an electrospray 
      ionization source in the positive mode (ESI+) for cyflumetofen and 
      2-(trifluoromethyl) benzamide (B-3) and the negative mode (ESI-) for 
      alpha,alpha,alpha-trifluoro-o-toluic acid (B-1). The entire method was validated by 
      evaluating the repeatability, linearity, precision, trueness, and matrix effect. 
      Average recoveries of the analytes were in the range of 79.3-117.6% with relative 
      standard deviation values below 7.6%. Limits of quantification (LOQs) ranged from 
      0.7 to 9.8mugkg(-1), which were lower than the maximum residue limits (MRLs) for 
      the cyflumetofen found in foods in Japan.
CI  - Copyright (c) 2013 Elsevier B.V. All rights reserved.
FAU - Li, Minmin
AU  - Li M
AD  - State Key Laboratory for Biology of Plant Diseases and Insect Pests, Institute of 
      Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, 
      China.
FAU - Liu, Xingang
AU  - Liu X
FAU - Dong, Fengshou
AU  - Dong F
FAU - Xu, Jun
AU  - Xu J
FAU - Kong, Zhiqiang
AU  - Kong Z
FAU - Li, Yuanbo
AU  - Li Y
FAU - Zheng, Yongquan
AU  - Zheng Y
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20130528
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Acetonitriles)
RN  - 0 (Nanotubes, Carbon)
RN  - 0 (Propionates)
RN  - 0 (Tea)
RN  - QJW6N27119 (cyflumetofen)
RN  - Z072SB282N (acetonitrile)
SB  - IM
MH  - Acetonitriles/chemistry
MH  - Adsorption
MH  - Animals
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Fishes
MH  - Food Analysis/*methods
MH  - Fruit/chemistry
MH  - Limit of Detection
MH  - Meat/analysis
MH  - Nanotubes, Carbon/*chemistry
MH  - Propionates/*analysis/chemistry/isolation & purification/metabolism
MH  - Reproducibility of Results
MH  - Solid Phase Extraction/*methods
MH  - Spectrometry, Mass, Electrospray Ionization
MH  - Swine
MH  - Tandem Mass Spectrometry/methods
MH  - Tea/chemistry
MH  - Vegetables/chemistry
OTO - NOTNLM
OT  - Animal origin
OT  - Cyflumetofen
OT  - Metabolites
OT  - Plant origin
OT  - UPLC-MS/MS
OT  - WMCNTs
EDAT- 2013/06/19 06:00
MHDA- 2014/01/22 06:00
CRDT- 2013/06/18 06:00
PHST- 2013/04/19 00:00 [received]
PHST- 2013/05/21 00:00 [revised]
PHST- 2013/05/22 00:00 [accepted]
PHST- 2013/06/18 06:00 [entrez]
PHST- 2013/06/19 06:00 [pubmed]
PHST- 2014/01/22 06:00 [medline]
AID - S0021-9673(13)00830-3 [pii]
AID - 10.1016/j.chroma.2013.05.052 [doi]
PST - ppublish
SO  - J Chromatogr A. 2013 Jul 26;1300:95-103. doi: 10.1016/j.chroma.2013.05.052. Epub 
      2013 May 28.