PMID- 24148394
OWN - NLM
STAT- MEDLINE
DCOM- 20140603
LR  - 20131023
IS  - 1873-3573 (Electronic)
IS  - 0039-9140 (Linking)
VI  - 116
DP  - 2013 Nov 15
TI  - Graphite furnace atomic absorption spectrometric detection of vanadium in water 
      and food samples after solid phase extraction on multiwalled carbon nanotubes.
PG  - 205-9
LID - S0039-9140(13)00443-8 [pii]
LID - 10.1016/j.talanta.2013.05.020 [doi]
AB  - Vanadium(V) ions as 8-hydroxyquinoline chelates were loaded on multiwalled carbon 
      nanotubes (MWNTs) in a mini chromatographic column. Vanadium was determined by 
      graphite furnace atomic absorption spectrometry (GFAAS). Various analytical 
      parameters including pH of the working solutions, amounts of 8-hydroxyquinoline, 
      eluent type, sample volume, and flow rates were investigated. The effects of 
      matrix ions and some transition metals were also studied. The column can be 
      reused 250 times without any loss in its sorption properties. The 
      preconcentration factor was found as 100. Detection limit (3 s) and limit of 
      quantification (10 s) for the vanadium in the optimal conditions were observed to 
      be 0.012 microg L(-1) and 0.040 mug L(-1), respectively. The capacity of adsorption 
      was 9.6 mg g(-1). Relative standard deviation (RSD) was found to be 5%. The 
      validation of the method was confirmed by using NIST SRM 1515 Apple leaves, NIST 
      SRM 1570a Spinach leaves and GBW 07605 Tea certified reference materials. The 
      procedure was applied to the determination of vanadium in tap water and bottled 
      drinking water samples. The procedure was also successfully applied to microwave 
      digested food samples including black tea, coffee, tomato, cabbage, zucchini, 
      apple and chicken samples.
CI  - Copyright (c) 2013 Elsevier B.V. All rights reserved.
FAU - Wadhwa, Sham Kumar
AU  - Wadhwa SK
AD  - Gaziosmanpasa University, Faculty of Science and Arts, Chemistry Department, 
      60250 Tokat, Turkey; National Centre of Excellence in Analytical Chemistry, 
      University of Sindh, Jamshoro 76080, Pakistan.
FAU - Tuzen, Mustafa
AU  - Tuzen M
FAU - Gul Kazi, Tasneem
AU  - Gul Kazi T
FAU - Soylak, Mustafa
AU  - Soylak M
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20130516
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
RN  - 0 (Environmental Pollutants)
RN  - 0 (Membranes, Artificial)
RN  - 0 (Nanotubes, Carbon)
RN  - 0 (Tea)
RN  - 00J9J9XKDE (Vanadium)
RN  - 5UTX5635HP (Oxyquinoline)
SB  - IM
MH  - Animals
MH  - Chickens
MH  - Environmental Pollutants/*isolation & purification
MH  - Equipment Reuse
MH  - Fresh Water/*chemistry
MH  - Humans
MH  - Hydrogen-Ion Concentration
MH  - Limit of Detection
MH  - Malus/chemistry
MH  - Meat/*analysis
MH  - Membranes, Artificial
MH  - Nanotubes, Carbon/chemistry
MH  - Oxyquinoline/chemistry
MH  - Plant Leaves/*chemistry
MH  - Reproducibility of Results
MH  - Solid Phase Extraction/*methods
MH  - Spectrophotometry, Atomic
MH  - Spinacia oleracea/chemistry
MH  - Tea/chemistry
MH  - Vanadium/*isolation & purification
OTO - NOTNLM
OT  - 8-hydroxyquinoline
OT  - Atomic absorption spectrometry
OT  - Multiwalled carbon nanotubes
OT  - Solid phase extraction
OT  - Vanadium
EDAT- 2013/10/24 06:00
MHDA- 2014/06/04 06:00
CRDT- 2013/10/24 06:00
PHST- 2013/04/09 00:00 [received]
PHST- 2013/05/04 00:00 [revised]
PHST- 2013/05/10 00:00 [accepted]
PHST- 2013/10/24 06:00 [entrez]
PHST- 2013/10/24 06:00 [pubmed]
PHST- 2014/06/04 06:00 [medline]
AID - S0039-9140(13)00443-8 [pii]
AID - 10.1016/j.talanta.2013.05.020 [doi]
PST - ppublish
SO  - Talanta. 2013 Nov 15;116:205-9. doi: 10.1016/j.talanta.2013.05.020. Epub 2013 May 
      16.