PMID- 24321764
OWN - NLM
STAT- MEDLINE
DCOM- 20140903
LR  - 20191210
IS  - 1873-376X (Electronic)
IS  - 1570-0232 (Linking)
VI  - 945-946
DP  - 2014 Jan 15
TI  - Determination of polybrominated diphenyl ethers and polychlorinated biphenyls in 
      fishery and aquaculture products using sequential solid phase extraction and 
      large volume injection gas chromatography/tandem mass spectrometry.
PG  - 75-83
LID - S1570-0232(13)00639-9 [pii]
LID - 10.1016/j.jchromb.2013.11.026 [doi]
AB  - A new method was developed to determine polybrominated diphenyl ethers (PBDEs) 
      and polychlorinated biphenyls (PCBs) in fishery and aquaculture products. Samples 
      were extracted by an accelerated solvent extraction system and cleaned up by 
      sequential solid phase extraction (SPE) including dispersive SPE (D-SPE) and 
      tandem SPE. PBDEs and PCBs were analyzed by a large-volume injection gas 
      chromatography triple quadrupole mass spectrometry (LVI-GC-QqQ-MS/MS). Good 
      linearity (R(2)>/=0.9958) was achieved. Method detection limits (MDLs) were 
      0.16-3.3pgg(-1) (wet weight, ww) for PBDEs and 0.13-0.97pgg(-1)ww for PCBs. Mean 
      recoveries were 60-140% with relative standard deviations (RSDs) of less than 20% 
      in weever fish, scallop and shrimp samples spiked at a lower level of 
      13-31pgg(-1)ww and a higher level of 50-125pgg(-1)ww. Certified reference 
      materials were analyzed with acceptable results. The method reduced solvent 
      consumption, analytical time and labor, and is suitable for the routine analysis 
      of PBDEs and PCBs in fishery and aquaculture products.
CI  - Copyright (c) 2013 Elsevier B.V. All rights reserved.
FAU - Lu, Dasheng
AU  - Lu D
AD  - Shanghai Municipal Center for Disease Control and Prevention, 1380 Zhongshan West 
      Road, Shanghai 200336, China.
FAU - Lin, Yuanjie
AU  - Lin Y
AD  - Shanghai Municipal Center for Disease Control and Prevention, 1380 Zhongshan West 
      Road, Shanghai 200336, China.
FAU - Feng, Chao
AU  - Feng C
AD  - Shanghai Municipal Center for Disease Control and Prevention, 1380 Zhongshan West 
      Road, Shanghai 200336, China.
FAU - Wang, Dongli
AU  - Wang D
AD  - California Department of Public Health, Richmond, CA 94804, USA.
FAU - Qiu, Xinlei
AU  - Qiu X
AD  - Shanghai Municipal Center for Disease Control and Prevention, 1380 Zhongshan West 
      Road, Shanghai 200336, China.
FAU - Jin, Yu'e
AU  - Jin Y
AD  - Shanghai Municipal Center for Disease Control and Prevention, 1380 Zhongshan West 
      Road, Shanghai 200336, China.
FAU - Xiong, Libei
AU  - Xiong L
AD  - Shanghai Municipal Center for Disease Control and Prevention, 1380 Zhongshan West 
      Road, Shanghai 200336, China.
FAU - Jin, Ying
AU  - Jin Y
AD  - School of Life Science, Shanghai University, Shanghai 200444, China.
FAU - Wang, Guoquan
AU  - Wang G
AD  - Shanghai Municipal Center for Disease Control and Prevention, 1380 Zhongshan West 
      Road, Shanghai 200336, China. Electronic address: gqwang@scdc.sh.cn.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PT  - Validation Study
DEP - 20131125
PL  - Netherlands
TA  - J Chromatogr B Analyt Technol Biomed Life Sci
JT  - Journal of chromatography. B, Analytical technologies in the biomedical and life 
      sciences
JID - 101139554
RN  - 0 (Halogenated Diphenyl Ethers)
RN  - 0 (Water Pollutants, Chemical)
RN  - DFC2HB4I0K (Polychlorinated Biphenyls)
SB  - IM
MH  - Animals
MH  - Fish Products/*analysis
MH  - Fisheries/methods
MH  - Fishes
MH  - Halogenated Diphenyl Ethers/*analysis
MH  - Hazard Analysis and Critical Control Points/*methods
MH  - Limit of Detection
MH  - Polychlorinated Biphenyls/*analysis
MH  - Solid Phase Extraction/*methods
MH  - Tandem Mass Spectrometry/methods
MH  - Water Pollutants, Chemical/*analysis
OTO - NOTNLM
OT  - Food safety
OT  - LVI-GC-QqQ-MS/MS
OT  - POPs
OT  - Tandem SPE
EDAT- 2013/12/11 06:00
MHDA- 2014/09/04 06:00
CRDT- 2013/12/11 06:00
PHST- 2013/06/25 00:00 [received]
PHST- 2013/11/11 00:00 [revised]
PHST- 2013/11/17 00:00 [accepted]
PHST- 2013/12/11 06:00 [entrez]
PHST- 2013/12/11 06:00 [pubmed]
PHST- 2014/09/04 06:00 [medline]
AID - S1570-0232(13)00639-9 [pii]
AID - 10.1016/j.jchromb.2013.11.026 [doi]
PST - ppublish
SO  - J Chromatogr B Analyt Technol Biomed Life Sci. 2014 Jan 15;945-946:75-83. doi: 
      10.1016/j.jchromb.2013.11.026. Epub 2013 Nov 25.