PMID- 24367455 OWN - NLM STAT- PubMed-not-MEDLINE DCOM- 20131224 LR - 20211021 IS - 1860-5397 (Print) IS - 1860-5397 (Electronic) IS - 1860-5397 (Linking) VI - 9 DP - 2013 TI - Synthesis of nucleotide-amino acid conjugates designed for photo-CIDNP experiments by a phosphotriester approach. PG - 2898-909 LID - 10.3762/bjoc.9.326 [doi] AB - Conjugates of 2'-deoxyguanosine, L-tryptophan and benzophenone designed to study pathways of fast radical reactions by the photo Chemically Induced Dynamic Nuclear Polarization (photo-CIDNP) method were obtained by the phosphotriester block liquid phase synthesis. The phosphotriester approach to the oligonucleotide synthesis was shown to be a versatile and economic strategy for preparing the required amount of high quality samples of nucleotide-amino acid conjugates. FAU - Abramova, Tatyana V AU - Abramova TV AD - Institute of Chemical Biology and Fundamental Medicine, SB RAS, Lavrent'ev Ave, 8, Novosibirsk 630090, Russia ; Novosibirsk State University, Pirogova St. 2, Novosibirsk 630090, Russia. FAU - Morozova, Olga B AU - Morozova OB AD - Novosibirsk State University, Pirogova St. 2, Novosibirsk 630090, Russia ; International Tomography Center, SB RAS, Institutskaya 3a, Novosibirsk 630090, Russia. FAU - Silnikov, Vladimir N AU - Silnikov VN AD - Institute of Chemical Biology and Fundamental Medicine, SB RAS, Lavrent'ev Ave, 8, Novosibirsk 630090, Russia. FAU - Yurkovskaya, Alexandra V AU - Yurkovskaya AV AD - Novosibirsk State University, Pirogova St. 2, Novosibirsk 630090, Russia ; International Tomography Center, SB RAS, Institutskaya 3a, Novosibirsk 630090, Russia. LA - eng PT - Journal Article DEP - 20131218 PL - Germany TA - Beilstein J Org Chem JT - Beilstein journal of organic chemistry JID - 101250746 PMC - PMC3869286 OTO - NOTNLM OT - CIDNP OT - nucleotide-amino acid conjugates OT - oligonucleotide synthesis OT - phosphotriester approach EDAT- 2013/12/25 06:00 MHDA- 2013/12/25 06:01 PMCR- 2013/12/18 CRDT- 2013/12/25 06:00 PHST- 2013/09/23 00:00 [received] PHST- 2013/11/15 00:00 [accepted] PHST- 2013/12/25 06:00 [entrez] PHST- 2013/12/25 06:00 [pubmed] PHST- 2013/12/25 06:01 [medline] PHST- 2013/12/18 00:00 [pmc-release] AID - 10.3762/bjoc.9.326 [doi] PST - epublish SO - Beilstein J Org Chem. 2013 Dec 18;9:2898-909. doi: 10.3762/bjoc.9.326. eCollection 2013.