PMID- 24401414
OWN - NLM
STAT- MEDLINE
DCOM- 20140902
LR  - 20140109
IS  - 1873-3573 (Electronic)
IS  - 0039-9140 (Linking)
VI  - 119
DP  - 2014 Feb
TI  - Determination of five pyrethroids in tea drinks by dispersive solid phase 
      extraction with polyaniline-coated magnetic particles.
PG  - 268-75
LID - S0039-9140(13)00881-3 [pii]
LID - 10.1016/j.talanta.2013.11.007 [doi]
AB  - The polyaniline-coated magnetic particles with bowl-shaped morphology 
      (Fe3O4/C/PANI microbowls) were successfully prepared and characterized by 
      scanning electron microscopy, transmission electron microscopy and vibrating 
      sample magnetometry. The prepared microbowls were used as the magnetic adsorbent 
      in dispersive solid phase extraction of five pyrethroids, including cyhalothrin, 
      beta-cypermethrin, esfenvalerate, permethrin and bifenthrin in plain tea drinks. 
      The effects of experiment factors, including amount of Fe3O4/C/PANI microbowls, 
      pH value, ultrasound extraction time and desorption conditions, were 
      investigated. The extraction recoveries obtained with 8 mg of magnetic microbowls 
      were satisfactory, and the microbowls can be reused after easy washing. Thus, a 
      simple, selective and effective method for the determination of the pyrethroids 
      was established successfully. The results showed that the method had good 
      linearity (r=0.9992-0.9998), and the limits of detections (LODs) were from 0.025 
      to 0.032 ng mL(-1). The intra-day and inter-day relative standard deviations 
      (RSDs) were in the range of 2.4-6.1% and 3.5-8.8%, respectively. Recoveries 
      obtained by analyzing the real tea drinks were in the range of 72.1-118.4%.
CI  - (c) 2013 Published by Elsevier B.V.
FAU - Wang, Yuanpeng
AU  - Wang Y
AD  - College of Chemistry, Jilin University, Qianjin Street 2699, Changchun 130012, PR 
      China.
FAU - Sun, Ying
AU  - Sun Y
AD  - College of Chemistry, Jilin University, Qianjin Street 2699, Changchun 130012, PR 
      China.
FAU - Gao, Yan
AU  - Gao Y
AD  - College of Chemistry, Jilin University, Qianjin Street 2699, Changchun 130012, PR 
      China.
FAU - Xu, Bo
AU  - Xu B
AD  - College of Chemistry, Jilin University, Qianjin Street 2699, Changchun 130012, PR 
      China.
FAU - Wu, Qiong
AU  - Wu Q
AD  - College of Chemistry, Jilin University, Qianjin Street 2699, Changchun 130012, PR 
      China.
FAU - Zhang, Hanqi
AU  - Zhang H
AD  - College of Chemistry, Jilin University, Qianjin Street 2699, Changchun 130012, PR 
      China.
FAU - Song, Daqian
AU  - Song D
AD  - College of Chemistry, Jilin University, Qianjin Street 2699, Changchun 130012, PR 
      China. Electronic address: songdq@jlu.edu.cn.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20131109
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
RN  - 0 (Aniline Compounds)
RN  - 0 (Pyrethrins)
RN  - 0 (Tea)
RN  - 0 (polyaniline)
SB  - IM
MH  - Aniline Compounds/*chemistry
MH  - Beverages/*analysis
MH  - Chromatography, Liquid/methods
MH  - *Magnetics
MH  - Microscopy, Electron, Scanning
MH  - Microscopy, Electron, Transmission
MH  - Pyrethrins/*analysis
MH  - Solid Phase Extraction/*methods
MH  - Spectrophotometry, Ultraviolet/methods
MH  - Tea/*chemistry
OTO - NOTNLM
OT  - Dispersive solid phase extraction
OT  - Polyaniline-coated magnetic microbowls
OT  - Pyrethroids
OT  - Tea drinks
OT  - Ultra fast liquid chromatography
EDAT- 2014/01/10 06:00
MHDA- 2014/09/03 06:00
CRDT- 2014/01/10 06:00
PHST- 2013/07/09 00:00 [received]
PHST- 2013/10/18 00:00 [revised]
PHST- 2013/11/01 00:00 [accepted]
PHST- 2014/01/10 06:00 [entrez]
PHST- 2014/01/10 06:00 [pubmed]
PHST- 2014/09/03 06:00 [medline]
AID - S0039-9140(13)00881-3 [pii]
AID - 10.1016/j.talanta.2013.11.007 [doi]
PST - ppublish
SO  - Talanta. 2014 Feb;119:268-75. doi: 10.1016/j.talanta.2013.11.007. Epub 2013 Nov 
      9.