PMID- 24411090
OWN - NLM
STAT- MEDLINE
DCOM- 20140710
LR  - 20181202
IS  - 1873-3778 (Electronic)
IS  - 0021-9673 (Linking)
VI  - 1328
DP  - 2014 Feb 7
TI  - Simultaneous determination of seven bisphenols in environmental water and solid 
      samples by liquid chromatography-electrospray tandem mass spectrometry.
PG  - 26-34
LID - S0021-9673(13)01975-4 [pii]
LID - 10.1016/j.chroma.2013.12.074 [doi]
AB  - This article presents a simple and universal analytical method for the 
      simultaneous analysis of bisphenol S (BPS), bisphenol F (BPF), bisphenol A (BPA), 
      bisphenol B (BPB), bisphenol AF (BPAF), tetrachlorobisphenol A (TCBPA), and 
      tetrabromobisphenol A (TBBPA) in environmental water (river water, sewage) and 
      solid samples (sediment, sludge) based on liquid chromatography-electrospray 
      tandem mass spectrometry (LC-MS/MS). Analytes were extracted from water samples 
      using hydrophilic lipophilic balanced (HLB) solid-phase extraction (SPE) 
      cartridges, and the extracts were further purified using MAX SPE cartridges. For 
      the solid samples, a combination of ultrasonic extraction with the same SPE 
      clean-up procedures used for the water samples was employed. The absolute 
      recoveries for all analytes in the water and solid samples ranged from 57.1 to 
      114.3%. Good method reproducibility was achieved in terms of intra- and inter-day 
      precision, yielding relative standard deviations (RSDs) less than 16.9 and 18.1%, 
      respectively. The method limits of quantitation (MLOQ) for the seven compounds in 
      environmental water and solid samples ranged from 0.05 to 4.35ng/L and from 0.06 
      to 2.83ng/g (dry weight, d.w.), respectively. Finally, this method was 
      successfully applied to real environmental sample analysis, which revealed that 
      all of the tested BPs were present, with the exception of BPB.
CI  - Copyright (c) 2014 Elsevier B.V. All rights reserved.
FAU - Yang, Yunjia
AU  - Yang Y
AD  - Beijing Key Laboratory of Diagnostic and Traceability Technologies for Food 
      Poisoning, Beijing Research Center for Preventive Medicine, Beijing 100013, 
      China.
FAU - Lu, Libin
AU  - Lu L
AD  - Beijing Key Laboratory of Diagnostic and Traceability Technologies for Food 
      Poisoning, Beijing Research Center for Preventive Medicine, Beijing 100013, 
      China.
FAU - Zhang, Jing
AU  - Zhang J
AD  - Beijing Key Laboratory of Diagnostic and Traceability Technologies for Food 
      Poisoning, Beijing Research Center for Preventive Medicine, Beijing 100013, 
      China.
FAU - Yang, Yi
AU  - Yang Y
AD  - Beijing Key Laboratory of Diagnostic and Traceability Technologies for Food 
      Poisoning, Beijing Research Center for Preventive Medicine, Beijing 100013, 
      China.
FAU - Wu, Yongning
AU  - Wu Y
AD  - Key Laboratory of Food Safety Risk Assessment, Ministry of Health and China 
      National Center for Food Safety and Risk Assessment, Beijing 100021, China.
FAU - Shao, Bing
AU  - Shao B
AD  - Beijing Key Laboratory of Diagnostic and Traceability Technologies for Food 
      Poisoning, Beijing Research Center for Preventive Medicine, Beijing 100013, 
      China. Electronic address: shaobingch@sina.com.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20131230
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Phenols)
RN  - 0 (Sewage)
RN  - 0 (Water Pollutants, Chemical)
SB  - IM
MH  - Chromatography, Liquid/methods
MH  - Fresh Water/*chemistry
MH  - Phenols/*analysis
MH  - Reproducibility of Results
MH  - Rivers
MH  - Sewage/*chemistry
MH  - Solid Phase Extraction
MH  - Spectrometry, Mass, Electrospray Ionization/methods
MH  - Tandem Mass Spectrometry/methods
MH  - Water Pollutants, Chemical/*analysis
OTO - NOTNLM
OT  - Bisphenols
OT  - Environmental water
OT  - Liquid chromatography-tandem mass spectrometry
OT  - Sludge
OT  - Solid-phase extraction
EDAT- 2014/01/15 06:00
MHDA- 2014/07/11 06:00
CRDT- 2014/01/14 06:00
PHST- 2013/08/12 00:00 [received]
PHST- 2013/12/21 00:00 [revised]
PHST- 2013/12/24 00:00 [accepted]
PHST- 2014/01/14 06:00 [entrez]
PHST- 2014/01/15 06:00 [pubmed]
PHST- 2014/07/11 06:00 [medline]
AID - S0021-9673(13)01975-4 [pii]
AID - 10.1016/j.chroma.2013.12.074 [doi]
PST - ppublish
SO  - J Chromatogr A. 2014 Feb 7;1328:26-34. doi: 10.1016/j.chroma.2013.12.074. Epub 
      2013 Dec 30.