PMID- 24417086
OWN - NLM
STAT- MEDLINE
DCOM- 20160125
LR  - 20190318
IS  - 0513-4870 (Print)
IS  - 0513-4870 (Linking)
VI  - 48
IP  - 10
DP  - 2013 Oct
TI  - [Sample pretreatment methods of pesticide residues in Panax notoginseng of 
      Chinese traditional medicine].
PG  - 1585-9
AB  - Two sample pretreatment methods of pesticide residues in Panax notoginseng of 
      Chinese traditional medicine were developed. For Method I, the residues were 
      extracted from homogenized tissue with n-hexane-dichloromethane (6:4) by means of 
      ultrasonication, the crude extract was purified by an Envi-carb/NH2 solid-phase 
      extraction (SPE) column. For Method II, matrix solid-phase dispersion (MSPD) 
      technique was used for extracting and cleaning up. The eluates were concentrated 
      by rotary evaporation, and then were redissolved in dichloromethane prior to 
      GC-MS determination. The determination was performed in selected ion monitoring 
      (SIM) mode with the external calibration for quantitative analysis. Under the 
      optimal conditions, the results indicated that the methods are easier and faster, 
      the recoveries of method I for the spiked standards at concentration of 0.01, 
      0.5, and 2.0 mg x kg(-1) were 81.90%-102.10% with the relative standard 
      deviations (RSDs) of 3.60%-7.10%. The recoveries of method II were 96.26%-104.20% 
      with the RSDs of 3.52%-7.94%. The detection limits (S/N) for residues of 
      pesticides were in the range of 0.48-1.34 ng x g(-1). The results indicated that 
      these multiresidue analysis methods can meet the requirements for determination 
      of residue pesticides and can be appropriate for trace analysis of residue 
      pesticides in Panax notoginseng.
FAU - Wu, Na
AU  - Wu N
AD  - Department of Chemistry, Honghe College, Mengzi 661100, China.
FAU - Liu, Wei
AU  - Liu W
AD  - Department of Chemistry, Honghe College, Mengzi 661100, China.
FAU - Yan, He-Ping
AU  - Yan HP
AD  - Department of Chemistry, Honghe College, Mengzi 661100, China.
FAU - Fan, Ai-Ping
AU  - Fan AP
AD  - Department of Chemistry, Honghe College, Mengzi 661100, China.
FAU - Huang, Du-Shu
AU  - Huang DS
AD  - Department of Chemistry, Honghe College, Mengzi 661100, China.
FAU - Zhou, Bo
AU  - Zhou B
AD  - Department of Chemistry, Honghe College, Mengzi 661100, China.
FAU - Chen, Xian-Lan
AU  - Chen XL
AD  - Department of Chemistry, Honghe College, Mengzi 661100, China.
FAU - Xu, Shi-Juan
AU  - Xu SJ
AD  - Department of Chemistry, Honghe College, Mengzi 661100, China.
FAU - Shi, Ling
AU  - Shi L
AD  - Department of Chemistry, Honghe College, Mengzi 661100, China.
LA  - chi
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Yao Xue Xue Bao
JT  - Yao xue xue bao = Acta pharmaceutica Sinica
JID - 21710340R
RN  - 0 (Hexanes)
RN  - 0 (Pesticide Residues)
RN  - 0 (Solvents)
RN  - 2DDG612ED8 (n-hexane)
RN  - 588X2YUY0A (Methylene Chloride)
SB  - IM
MH  - Analytic Sample Preparation Methods/*methods
MH  - Gas Chromatography-Mass Spectrometry
MH  - Hexanes/chemistry
MH  - Methylene Chloride/chemistry
MH  - Panax notoginseng/*chemistry
MH  - Pesticide Residues/*analysis
MH  - *Solid Phase Extraction
MH  - Solvents
EDAT- 2014/01/15 06:00
MHDA- 2016/01/26 06:00
CRDT- 2014/01/15 06:00
PHST- 2014/01/15 06:00 [entrez]
PHST- 2014/01/15 06:00 [pubmed]
PHST- 2016/01/26 06:00 [medline]
PST - ppublish
SO  - Yao Xue Xue Bao. 2013 Oct;48(10):1585-9.