PMID- 24558844
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20150708
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 31
IP  - 11
DP  - 2013 Nov
TI  - [Determination of 21 phenolic compounds in soil by ultrasonic extraction-gas 
      chromatography].
PG  - 1081-6
AB  - An effective method was developed to determine phenolic compounds in soil by 
      ultrasonic extraction-gas chromatography (GC). The soil sample was extracted with 
      methylene dichloride-hexane (2:1, v/v) for 3 min with the extraction temperature 
      lower than 50 degrees C for 3 times. The extract was purified by alkaline aqueous 
      solution (pH > 12), and the phenolic compounds were dissolved in aqueous 
      solution. After the organic solution was discarded, the aqueous solution was 
      adjusted to pH <3 and subsequently extracted with methylene dichloride-ethyl 
      acetate (4:1, v/v) twice. The analytes were determined by GC-FID and quantified 
      by external standard method. The limits of quantification for all tested phenolic 
      compounds were 0.01-0.06 mg/kg in about 10 g soil samples. The recoveries were 
      between 62.9% and 111.4% with the relative standard deviations (RSDs) in the 
      range of 4.3%-24.0% (n = 6). The results showed that this method is sensitive, 
      accurate, and suitable for the determination of the 21 phenolic compounds in 
      soil.
FAU - Yang, Lili
AU  - Yang L
AD  - Nanjing Environmental Monitoring Center, Nanjing 210013, China. yllyj@126.com
FAU - Wang, Meifei
AU  - Wang M
AD  - Nanjing Environmental Monitoring Center, Nanjing 210013, China.
FAU - Hu, Enyu
AU  - Hu E
AD  - Nanjing Environmental Monitoring Center, Nanjing 210013, China.
FAU - Liu, Jing
AU  - Liu J
AD  - Nanjing Environmental Monitoring Center, Nanjing 210013, China.
FAU - Wu, Lijuan
AU  - Wu L
AD  - Nanjing Environmental Monitoring Center, Nanjing 210013, China.
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2014/02/25 06:00
MHDA- 2014/02/25 06:01
CRDT- 2014/02/25 06:00
PHST- 2014/02/25 06:00 [entrez]
PHST- 2014/02/25 06:00 [pubmed]
PHST- 2014/02/25 06:01 [medline]
AID - 10.3724/sp.j.1123.2013.05005 [doi]
PST - ppublish
SO  - Se Pu. 2013 Nov;31(11):1081-6. doi: 10.3724/sp.j.1123.2013.05005.