PMID- 24558846
OWN - NLM
STAT- MEDLINE
DCOM- 20150708
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 31
IP  - 11
DP  - 2013 Nov
TI  - [Determination of alditols in foods by ion chromatography-mass spectrometry].
PG  - 1093-101
AB  - A method for the determination of alditols in foods by ion chromatography-mass 
      spectrometry (IC-MS) has been developed. The samples were extracted and cleaned 
      up with the solid phase extraction (SPE). Then, the ion chromatographic 
      separation was performed on a CarboPar MA1 column. The alditols were determined 
      by MS with the selected ion monitoring (SIM) mode and quantified by the external 
      standard method. The calibration curves showed good linearity in the certain 
      ranges with the correlation coefficients (R2) greater than 0.99. The limits of 
      quantification (S/N = 10) of erythritol, xylitol, D-sorbitol, D-mannitol, 
      lactitol, maltitol were 0.98, 1.99, 2.24, 5.92, 13.56, 13.21 mg/kg and the limits 
      of detection (S/N = 3) were 0.28, 0.59, 0.71, 1.74, 4.14, 4.03 mg/kg, 
      respectively. The spiked recoveries of the alditols in the foods at different 
      levels were in the range of 82.5%-108.0% with the relative standard deviations 
      (RSDs) of 1.5%-7.6%. The sensitivity, accuracy and precision of the method meet 
      the technical standards of the determination. The method can be applied to the 
      determination of alditols in foods.
FAU - Zhou, Hongbin
AU  - Zhou H
AD  - State Key Laboratory of Food Additive and Condiment Testing, Zhenjiang 212008, 
      China.
FAU - Xiong, Zhiyu
AU  - Xiong Z
AD  - State Key Laboratory of Food Additive and Condiment Testing, Zhenjiang 212008, 
      China.
FAU - Li, Ping
AU  - Li P
AD  - State Key Laboratory of Food Additive and Condiment Testing, Zhenjiang 212008, 
      China.
FAU - Li, Jing
AU  - Li J
AD  - State Key Laboratory of Food Additive and Condiment Testing, Zhenjiang 212008, 
      China.
FAU - Sun, Li
AU  - Sun L
AD  - State Key Laboratory of Food Additive and Condiment Testing, Zhenjiang 212008, 
      China.
FAU - Zhao, Yunxia
AU  - Zhao Y
AD  - State Key Laboratory of Food Additive and Condiment Testing, Zhenjiang 212008, 
      China.
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Sugar Alcohols)
SB  - IM
MH  - *Food Analysis
MH  - *Gas Chromatography-Mass Spectrometry
MH  - Solid Phase Extraction
MH  - Sugar Alcohols/*analysis
MH  - Tandem Mass Spectrometry
EDAT- 2014/02/25 06:00
MHDA- 2015/07/15 06:00
CRDT- 2014/02/25 06:00
PHST- 2014/02/25 06:00 [entrez]
PHST- 2014/02/25 06:00 [pubmed]
PHST- 2015/07/15 06:00 [medline]
AID - 10.3724/sp.j.1123.2013.05008 [doi]
PST - ppublish
SO  - Se Pu. 2013 Nov;31(11):1093-101. doi: 10.3724/sp.j.1123.2013.05008.