PMID- 24669710
OWN - NLM
STAT- MEDLINE
DCOM- 20150708
LR  - 20231213
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 31
IP  - 12
DP  - 2013 Dec
TI  - [Simultaneous determination of five Amadori compounds in tobacco by high 
      performance liquid chromatography-mass spectrometry].
PG  - 1189-93
AB  - A method of high performance liquid chromatography-triple quadrupole mass 
      spectrometry (HPLC-QqQ MS) in multiple reaction monitoring (MRM) mode for 
      simultaneous determination of five Amadori compounds in tobacco has been 
      developed. The separation was performed on an XBridge Amide column (250 mm x 4.6 
      mm, 3.5 microm) by gradient elution using methanol and water as mobile phases. 
      The linearity of this method was good with the correlation coefficients (r) of 
      0.9895-0.9989. The limits of detection (S/N = 3) were from 3.51 microg/L to 14.86 
      microg/L, and the limits of quantitation (S/N = 10) were from 10.18 microg/L to 
      44.58 microg/L. The recoveries varied from 92.6% to 123.6% with the relative 
      standard deviations (RSDs) less than 9.4%. The established method is rapid, 
      accurate, robust and convenient, and it could be applied to the measurement of 
      the five Amadori compounds in tobacco and cigarettes.
FAU - Wang, Hongrui
AU  - Wang H
FAU - Xie, Yuanyuan
AU  - Xie Y
FAU - Liang, Qionglin
AU  - Liang Q
FAU - Wang, Yiming
AU  - Wang Y
FAU - Hu, Ping
AU  - Hu P
FAU - Luo, Guoan
AU  - Luo G
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
SB  - IM
MH  - *Chromatography, High Pressure Liquid
MH  - *Tandem Mass Spectrometry
MH  - Nicotiana/*chemistry
EDAT- 2014/03/29 06:00
MHDA- 2015/07/15 06:00
CRDT- 2014/03/28 06:00
PHST- 2014/03/28 06:00 [entrez]
PHST- 2014/03/29 06:00 [pubmed]
PHST- 2015/07/15 06:00 [medline]
AID - 10.3724/sp.j.1123.2013.06029 [doi]
PST - ppublish
SO  - Se Pu. 2013 Dec;31(12):1189-93. doi: 10.3724/sp.j.1123.2013.06029.