PMID- 24779906
OWN - NLM
STAT- MEDLINE
DCOM- 20141219
LR  - 20191210
IS  - 1939-3229 (Electronic)
IS  - 1939-3210 (Linking)
VI  - 6
IP  - 3
DP  - 2013
TI  - LC-TOF/MS determination of phthalates in edible salts from food markets in Korea.
PG  - 203-8
LID - 10.1080/19393210.2013.795194 [doi]
AB  - Residual quantities of 12 phthalates have been monitored in edible salts (raw 
      salts, refined salts, refined salts with additives and baked salts) available in 
      Korean food markets. Liquid-liquid extraction followed by liquid chromatography 
      time-of-flight mass spectrometry (LC-TOF/MS) was used to analyse the samples. The 
      method was validated and showed linear correlation (R(2) > 0.996) in the range 
      0.5-100 ng g(-)(1) for all target analytes. Recoveries were 85.9-108.4%, except for 
      diethyl phthalate (DEP). Relative standard deviations (RSDs) were 2.7-6.0% and 
      the limits of detection (LODs) were 1.2-2.8 ng g(-)(1). Although the contamination of 
      phthalates in salt would be trivial in comparison to those of other main foods 
      and below the reference dose of the Chronic Oral Exposure recommended by US-EPA, 
      the availability of reference data could be valuable for food chemists and salt 
      manufacturers.
FAU - Dirwono, Warnadi
AU  - Dirwono W
AD  - a Advanced Analysis Center , Korea Institute of Science and Technology , Seoul , 
      136-791 , Korea.
FAU - Nam, Yun Sik
AU  - Nam YS
FAU - Park, Hyun-Mee
AU  - Park HM
FAU - Lee, Kang-Bong
AU  - Lee KB
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
PT  - Validation Study
DEP - 20130723
PL  - England
TA  - Food Addit Contam Part B Surveill
JT  - Food additives & contaminants. Part B, Surveillance
JID - 101317183
RN  - 0 (Endocrine Disruptors)
RN  - 0 (Environmental Pollutants)
RN  - 0 (Food Additives)
RN  - 0 (Phthalic Acids)
RN  - 0 (Plasticizers)
SB  - IM
MH  - Chromatography, High Pressure Liquid
MH  - Condiments/*analysis/economics/standards
MH  - Diet/ethnology
MH  - Endocrine Disruptors/*analysis/chemistry
MH  - Environmental Pollutants/*analysis/chemistry
MH  - Food Additives
MH  - *Food Contamination
MH  - Food Handling
MH  - Food Inspection/*methods
MH  - Guideline Adherence
MH  - Health Policy
MH  - Health Promotion
MH  - Humans
MH  - Liquid-Liquid Extraction
MH  - Phthalic Acids/*analysis/chemistry
MH  - Plasticizers/*analysis/chemistry
MH  - Republic of Korea
MH  - Spectrometry, Mass, Electrospray Ionization
MH  - United States
MH  - United States Environmental Protection Agency
OTO - NOTNLM
OT  - LC-TOF/MS
OT  - baked salt
OT  - edible salt
OT  - phthalate
OT  - unrefined raw salt
EDAT- 2014/05/02 06:00
MHDA- 2014/12/20 06:00
CRDT- 2014/05/01 06:00
PHST- 2014/05/01 06:00 [entrez]
PHST- 2014/05/02 06:00 [pubmed]
PHST- 2014/12/20 06:00 [medline]
AID - 10.1080/19393210.2013.795194 [doi]
PST - ppublish
SO  - Food Addit Contam Part B Surveill. 2013;6(3):203-8. doi: 
      10.1080/19393210.2013.795194. Epub 2013 Jul 23.