PMID- 24780256
OWN - NLM
STAT- MEDLINE
DCOM- 20141014
LR  - 20181202
IS  - 1873-3778 (Electronic)
IS  - 0021-9673 (Linking)
VI  - 1345
DP  - 2014 Jun 6
TI  - Fast determination of 22 sulfonamides from chicken breast muscle using core-shell 
      nanoring amino-functionalized superparamagnetic molecularly imprinted polymer 
      followed by liquid chromatography-tandem mass spectrometry.
PG  - 17-28
LID - S0021-9673(14)00580-9 [pii]
LID - 10.1016/j.chroma.2014.04.028 [doi]
AB  - A novel, simple and sensitive method was developed for the simultaneous 
      determination of 22 sulfonamides (SAs) in chicken breast muscle by using the 
      dispersive micro-solid-phase extraction (d-mu-SPE) procedure combined with 
      ultra-fast liquid chromatography-tandem quadrupole mass spectrometry 
      (UFLC-MS/MS). The excellent core-shell nanoring amino-functionalized 
      superparamagnetic molecularly imprinted polymer (CS-NR-Mag-MIP) was used as 
      sorbent, and the main factors affecting the extraction efficiency were 
      investigated in detail. All target compounds showed good linearities in the 
      tested range with correlation coefficients (r) higher than 0.9980. The mean 
      recoveries were in the range of 85.0-112.2% at low, medium and high concentration 
      levels (0.1, 1.0 and 5.0 ng/g). The intra-day and inter-day relative standard 
      deviations (RSDs) were lower than 6.0% and 8.9%, respectively. The limits of 
      quantification for the 22 SAs were between 0.013 and 0.099 ng/g. The developed 
      d-mu-SPE-UFLC-MS/MS method had been successfully applied to the chicken breast 
      muscle samples for food-safety risk monitoring in Zhejiang Province, China. The 
      results showed sulfamethazine, sulfamethoxazole and sulfaquinoxaline in five out 
      of three hundred collected samples were detected with concentrations of 
      0.418-2.28, 16.4 and 2.93 ng/g, respectively. It was confirmed that the 
      CS-NR-Mag-MIP was a kind of highly effective d-mu-SPE materials used for the SAs 
      analyses.
CI  - Copyright (c) 2014 Elsevier B.V. All rights reserved.
FAU - Zhao, Yong-Gang
AU  - Zhao YG
AD  - Zhejiang Provincial Key Laboratory of Health Risk Appraisal for Trace Toxic 
      Chemicals, Ningbo Municipal Center for Disease Control and Prevention, Ningbo, 
      Zhejiang 315010, China; Ningbo Key Laboratory of Poison Research and Control, 
      Ningbo Municipal Center for Disease Control and Prevention, Ningbo, Zhejiang 
      315010, China.
FAU - Zhou, Li-Xin
AU  - Zhou LX
AD  - Medical School, Ningbo University, Ningbo, Zhejiang 315211, China.
FAU - Pan, Sheng-Dong
AU  - Pan SD
AD  - Zhejiang Provincial Key Laboratory of Health Risk Appraisal for Trace Toxic 
      Chemicals, Ningbo Municipal Center for Disease Control and Prevention, Ningbo, 
      Zhejiang 315010, China; Ningbo Key Laboratory of Poison Research and Control, 
      Ningbo Municipal Center for Disease Control and Prevention, Ningbo, Zhejiang 
      315010, China.
FAU - Zhan, Ping-Ping
AU  - Zhan PP
AD  - School of Marine Sciences, Ningbo University, Ningbo, Zhejiang 315211, China.
FAU - Chen, Xiao-Hong
AU  - Chen XH
AD  - Zhejiang Provincial Key Laboratory of Health Risk Appraisal for Trace Toxic 
      Chemicals, Ningbo Municipal Center for Disease Control and Prevention, Ningbo, 
      Zhejiang 315010, China; Ningbo Key Laboratory of Poison Research and Control, 
      Ningbo Municipal Center for Disease Control and Prevention, Ningbo, Zhejiang 
      315010, China.
FAU - Jin, Mi-Cong
AU  - Jin MC
AD  - Zhejiang Provincial Key Laboratory of Health Risk Appraisal for Trace Toxic 
      Chemicals, Ningbo Municipal Center for Disease Control and Prevention, Ningbo, 
      Zhejiang 315010, China; Ningbo Key Laboratory of Poison Research and Control, 
      Ningbo Municipal Center for Disease Control and Prevention, Ningbo, Zhejiang 
      315010, China. Electronic address: jmcjc@163.com.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20140418
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Ferric Compounds)
RN  - 0 (Magnetite Nanoparticles)
RN  - 0 (Polymers)
RN  - 0 (Sulfonamides)
RN  - 1K09F3G675 (ferric oxide)
SB  - IM
MH  - Animals
MH  - Chickens
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Ferric Compounds/*chemistry
MH  - Liquid Phase Microextraction/methods
MH  - Magnetite Nanoparticles/chemistry/ultrastructure
MH  - Meat/*analysis
MH  - Metal Nanoparticles/chemistry/ultrastructure
MH  - Molecular Imprinting/*methods
MH  - Muscle, Skeletal/*chemistry
MH  - Polymers/chemistry
MH  - Sulfonamides/*analysis
MH  - Tandem Mass Spectrometry/*methods
MH  - Time Factors
OTO - NOTNLM
OT  - Chicken breast muscle
OT  - Core-shell nanoring amino-functionalized superparamagnetic molecularly imprinted 
      polymer (CS-NR-Mag-MIP)
OT  - Dispersive micro-solid-phase extraction (d-mu-SPE)
OT  - Matrix effect
OT  - Sulfonamides
OT  - Ultra-fast liquid chromatography-tandem quadrupole mass spectrometry (UFLC-MS/MS)
EDAT- 2014/05/02 06:00
MHDA- 2014/10/15 06:00
CRDT- 2014/05/01 06:00
PHST- 2014/01/09 00:00 [received]
PHST- 2014/04/06 00:00 [revised]
PHST- 2014/04/09 00:00 [accepted]
PHST- 2014/05/01 06:00 [entrez]
PHST- 2014/05/02 06:00 [pubmed]
PHST- 2014/10/15 06:00 [medline]
AID - S0021-9673(14)00580-9 [pii]
AID - 10.1016/j.chroma.2014.04.028 [doi]
PST - ppublish
SO  - J Chromatogr A. 2014 Jun 6;1345:17-28. doi: 10.1016/j.chroma.2014.04.028. Epub 
      2014 Apr 18.