PMID- 24799252 OWN - NLM STAT- MEDLINE DCOM- 20150520 LR - 20181202 IS - 1873-7072 (Electronic) IS - 0308-8146 (Linking) VI - 160 DP - 2014 Oct 1 TI - Pesticide residues in fruits and vegetables from the Aegean region, Turkey. PG - 379-92 LID - S0308-8146(14)00226-X [pii] LID - 10.1016/j.foodchem.2014.02.051 [doi] AB - The purpose of this study was to investigate pesticide residues in fruits and vegetables from the Aegean region of Turkey. A total of 1423 samples of fresh fruit and vegetables were collected from 2010 to 2012. The samples were analysed to determine the concentrations of 186 pesticide residues. The analyses utilized ultrahigh performance liquid chromatography coupled with tandem mass spectrometry (UPLC/MS/MS) and gas chromatography with an electron capture detector (GC-ECD) confirmed by gas chromatography with mass spectrometry (GC-MS) after a multi-residue extraction procedure (the QuEChERS method). The results were evaluated according to maximum residue limits (MRLs) for each commodity and pesticide by Turkish Regulation. All pomegranate, cauliflower and cabbage samples were pesticides-free. A total of 754 samples contained detectable residues at or below MRLs, and 48 (8.4%) of the fruit samples and 83 (9.8%) of the vegetable samples contained pesticide residues above MRLs. MRL values were most often exceeded in arugula, cucumber, lemon, and grape commodities. All detected pesticides in apricot, carrot, kiwifruit and leek were below the MRLs. Acetamiprid, chlorpyriphos and carbendazim were the most detected pesticide residues. CI - Copyright (c) 2014 Elsevier Ltd. All rights reserved. FAU - Bakirci, Gozde Turkoz AU - Bakirci GT AD - Food Control and Research Laboratory, Aybak Natura, Izmir, Turkey. Electronic address: gozde.turkoz@naturalab.com.tr. FAU - Yaman Acay, Dilek Bengu AU - Yaman Acay DB AD - Food Control and Research Laboratory, Aybak Natura, Izmir, Turkey. Electronic address: bengu.yaman@naturalab.com.tr. FAU - Bakirci, Fatih AU - Bakirci F AD - Food Control and Research Laboratory, Aybak Natura, Izmir, Turkey. Electronic address: fatih.bakirci@naturalab.com.tr. FAU - Otles, Semih AU - Otles S AD - Department of Food Engineering, Ege University, 35100 Izmir, Bornova, Turkey. Electronic address: semih.otles@ege.edu.tr. LA - eng PT - Journal Article DEP - 20140222 PL - England TA - Food Chem JT - Food chemistry JID - 7702639 RN - 0 (Pesticide Residues) SB - IM MH - Chromatography, Gas MH - Food Contamination/*analysis MH - Fruit/*chemistry MH - Pesticide Residues/*analysis MH - Tandem Mass Spectrometry/methods MH - Turkey MH - Vegetables/*chemistry OTO - NOTNLM OT - Fruits and vegetables OT - GC-ECD/GC-MS OT - Pesticides residues OT - UPLC-MS/MS EDAT- 2014/05/07 06:00 MHDA- 2015/05/21 06:00 CRDT- 2014/05/07 06:00 PHST- 2013/09/30 00:00 [received] PHST- 2014/02/09 00:00 [revised] PHST- 2014/02/12 00:00 [accepted] PHST- 2014/05/07 06:00 [entrez] PHST- 2014/05/07 06:00 [pubmed] PHST- 2015/05/21 06:00 [medline] AID - S0308-8146(14)00226-X [pii] AID - 10.1016/j.foodchem.2014.02.051 [doi] PST - ppublish SO - Food Chem. 2014 Oct 1;160:379-92. doi: 10.1016/j.foodchem.2014.02.051. Epub 2014 Feb 22.