PMID- 24822450
OWN - NLM
STAT- MEDLINE
DCOM- 20150901
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 32
IP  - 2
DP  - 2014 Feb
TI  - [Determination of 14 pesticide residues in crucian carp using on-line gel 
      permeation chromatography-multi gas chromatography/mass spectrometry].
PG  - 157-61
AB  - A new method was developed for the determination of pesticide residues in crucian 
      carp using on-line gel permeation chromatography-multi gas chromatography/mass 
      spectrometry (GPC-MDGC/MS). The pesticide residues were extracted with 
      cyclohexane-ethyl acetate (1:1, v/v) for twice. After being frozen, the extract 
      was filtered by 0.22 microm member, and then cleaned up and analyzed by online 
      GPC-MDGC/MS. The pesticides were selectively transferred from the 1st column to 
      the 2nd column by means of heart cutting. As a result, selective transfers of 
      some pesticides from the first to the second dimension were at times essential to 
      avoid overlapping. The selected separation conditions from the study with 
      standards were applied to crucian carp spiked with some pesticide standards. The 
      performance of this method was examined by recovery, linearity and precision. 
      Inter-standard quantitative method was used for calculation. Good linear 
      relationship was achieved in the range of 0.01-0.9 mg/L for the 14 pesticides 
      with correlation coefficients above 0.99. The recoveries of the method ranged 
      from 83.0% to 112.9% with the relative standard deviations (RSDs) among 
      3.2%-12.0% at 3 spiked levels of 0.01, 0.05 and 0.1 mg/kg. This is a simple, 
      rapid method for the analysis of multiple pesticide residues in crucian carp with 
      high accuracy and sensitivity. The results prove that the employment of a 
      multidimensional analysis technique permits to avoid interferences of the 
      analytes with matrix components.
FAU - Li, Shujing
AU  - Li S
FAU - Dong, Mei
AU  - Dong M
FAU - Xu, Hong
AU  - Xu H
FAU - Mi, Jiebo
AU  - Mi J
FAU - Chen, Qiyong
AU  - Chen Q
FAU - Ge, Baokun
AU  - Ge B
FAU - Zhai, Ziqin
AU  - Zhai Z
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Pesticide Residues)
SB  - IM
MH  - Animals
MH  - *Carps
MH  - Gas Chromatography-Mass Spectrometry
MH  - Pesticide Residues/*analysis
MH  - Reference Standards
EDAT- 2014/05/16 06:00
MHDA- 2015/09/02 06:00
CRDT- 2014/05/15 06:00
PHST- 2014/05/15 06:00 [entrez]
PHST- 2014/05/16 06:00 [pubmed]
PHST- 2015/09/02 06:00 [medline]
AID - 10.3724/sp.j.1123.2013.10016 [doi]
PST - ppublish
SO  - Se Pu. 2014 Feb;32(2):157-61. doi: 10.3724/sp.j.1123.2013.10016.