PMID- 24961858
OWN - NLM
STAT- MEDLINE
DCOM- 20140911
LR  - 20180608
IS  - 0895-3988 (Print)
IS  - 0895-3988 (Linking)
VI  - 27
IP  - 6
DP  - 2014 Jun
TI  - Simultaneous determination of bisphenols and alkylphenols in water by solid phase 
      extraction and ultra performance liquid chromatography-tandem mass spectrometry.
PG  - 471-4
LID - 10.3967/bes2014.076 [doi]
AB  - To establish an analytical method for determination of four bisphenols (BPA, BPB, 
      BPF, and BPS) and two alkylphenols (4-n-OP, 4-n-NP) in water by ultra performance 
      liquid chromatography- tandem mass spectrometry (UPLC/MS/MS). The water samples 
      were extracted and condensed with solid-phase extraction (SPE) using C18 
      cartridges and eluted by acetonitrile. Separation was carried out with Acquity 
      BEH C8 column and detection were performed by UPLC/MS/MS. Quantification was 
      calculated by using the internal standard BPA-d16 and 4-n-NP-d8. The linear 
      correlation coefficients of these compounds in the range of 1.0-100.0 mug/L were 
      all over 0.999. The minimum detectable concentrations were 0.75-1.0 ng/L, and the 
      recoveries ranged from 87.0% to 106.9%. Relative standard deviations (RSDs) were 
      between 1.26% and 3.67%. Applying this method to detect the source water of 
      Chaohu Lake and drinking water of Hefei, six target compounds were detected in 
      different levels. This method is simple with high sensitivity and selectivity, 
      could be suitable for the determination of these compounds in source and drinking 
      water.
CI  - Copyright (c) 2014 The Editorial Board of Biomedical and Environmental Sciences. 
      Published by China CDC. All rights reserved.
FAU - Shan, Xiao Mei
AU  - Shan XM
AD  - Anhui Provincial Center for Disease Control and Prevention, Hefei 230601, Anhui, 
      China; School of Public Health, Anhui Medical University, Hefei 230032, Anhui, 
      China.
FAU - Shen, Deng Hui
AU  - Shen DH
AD  - School of Public Health, Anhui Medical University, Hefei 230032, Anhui, China.
FAU - Wang, Bing Shuang
AU  - Wang BS
AD  - School of Public Health, Anhui Medical University, Hefei 230032, Anhui, China.
FAU - Lu, Bei Bei
AU  - Lu BB
AD  - Ningbo City Center for Disease Control and Prevention, Ningbo 315010, Zhejiang, 
      China.
FAU - Huang, Fa Yuan
AU  - Huang FY
AD  - Anhui Provincial Center for Disease Control and Prevention, Hefei 230601, Anhui, 
      China.
LA  - eng
PT  - Letter
PT  - Research Support, Non-U.S. Gov't
PL  - China
TA  - Biomed Environ Sci
JT  - Biomedical and environmental sciences : BES
JID - 8909524
RN  - 0 (Endocrine Disruptors)
RN  - 0 (Phenols)
RN  - 0 (Water Pollutants, Chemical)
SB  - IM
MH  - Chromatography, Liquid
MH  - Endocrine Disruptors/*analysis
MH  - Phenols/*analysis
MH  - Solid Phase Extraction
MH  - Tandem Mass Spectrometry
MH  - Water Pollutants, Chemical/*analysis
EDAT- 2014/06/26 06:00
MHDA- 2014/09/12 06:00
CRDT- 2014/06/26 06:00
PHST- 2013/12/26 00:00 [received]
PHST- 2014/03/25 00:00 [accepted]
PHST- 2014/06/26 06:00 [entrez]
PHST- 2014/06/26 06:00 [pubmed]
PHST- 2014/09/12 06:00 [medline]
AID - S0895-3988(14)60071-4 [pii]
AID - 10.3967/bes2014.076 [doi]
PST - ppublish
SO  - Biomed Environ Sci. 2014 Jun;27(6):471-4. doi: 10.3967/bes2014.076.