PMID- 25062509
OWN - NLM
STAT- MEDLINE
DCOM- 20150511
LR  - 20140823
IS  - 1873-376X (Electronic)
IS  - 1570-0232 (Linking)
VI  - 967
DP  - 2014 Sep 15
TI  - Simultaneous determination of 50 residual pesticides in Flos Chrysanthemi using 
      accelerated solvent extraction and gas chromatography.
PG  - 1-7
LID - S1570-0232(14)00165-2 [pii]
LID - 10.1016/j.jchromb.2014.03.003 [doi]
AB  - A gas chromatographic method for simultaneous determination of 50 organochlorine 
      (OCP) and pyrethroid (PP) pesticides in Flos Chrysanthemi was established. 
      Accelerated solvent extraction (ASE) technique was used to extract the target 
      compounds, cleaned with alumina neutral-florisil column, and eluted by mixed 
      solvents of ethyl acetate and hexane (15:85, v/v). Selected pesticides were 
      identified using HP-5 and DB1701 capillary dual column and detected by 
      electron-capture detector. Quantitative analysis was performed using an external 
      standard by HP-5 capillary column. Results showed that recoveries were 
      73.4-120.1%, and the relative standard deviations (RSDs) were 1.6-12.4%. The 
      limits of detection of the method were 0.0021-0.0069 mg/kg, and the limits of 
      quantity were 0.0064-0.0210 mg/kg.
CI  - Copyright (c) 2014 Elsevier B.V. All rights reserved.
FAU - Huang, Xiaohui
AU  - Huang X
AD  - Department of Pharmacy, Xinhua Hospital, Shanghai Jiao tong University School of 
      Medicine, Shanghai 200092, China.
FAU - Zhao, Xinghui
AU  - Zhao X
AD  - Department of Pharmacy, Xuzhou Children's Hospital, Xuzhou 221000, China.
FAU - Lu, Xiaotong
AU  - Lu X
AD  - Department of Pharmacy, Xinhua Hospital, Shanghai Jiao tong University School of 
      Medicine, Shanghai 200092, China.
FAU - Tian, Huaiping
AU  - Tian H
AD  - Department of Pharmacy, Xinhua Hospital, Shanghai Jiao tong University School of 
      Medicine, Shanghai 200092, China.
FAU - Xu, Ajing
AU  - Xu A
AD  - Department of Pharmacy, Xinhua Hospital, Shanghai Jiao tong University School of 
      Medicine, Shanghai 200092, China.
FAU - Liu, Yan
AU  - Liu Y
AD  - Department of Pharmacy, Xinhua Hospital, Shanghai Jiao tong University School of 
      Medicine, Shanghai 200092, China.
FAU - Jian, Zhang
AU  - Jian Z
AD  - Department of Pharmacy, Xinhua Hospital, Shanghai Jiao tong University School of 
      Medicine, Shanghai 200092, China. Electronic address: zj_boss@126.com.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20140312
PL  - Netherlands
TA  - J Chromatogr B Analyt Technol Biomed Life Sci
JT  - Journal of chromatography. B, Analytical technologies in the biomedical and life 
      sciences
JID - 101139554
RN  - 0 (Drugs, Chinese Herbal)
RN  - 0 (Hydrocarbons, Chlorinated)
RN  - 0 (Pesticide Residues)
RN  - 0 (Pyrethrins)
SB  - IM
MH  - Chromatography, Gas/*methods
MH  - Drugs, Chinese Herbal/*chemistry
MH  - Hydrocarbons, Chlorinated/analysis/chemistry/isolation & purification
MH  - Limit of Detection
MH  - Linear Models
MH  - Pesticide Residues/*analysis/chemistry/isolation & purification
MH  - Pyrethrins/analysis/chemistry/isolation & purification
MH  - Reproducibility of Results
MH  - Solid Phase Extraction
OTO - NOTNLM
OT  - Flos Chrysanthemi
OT  - Gas chromatography
OT  - Multi-residues
OT  - Organochlorine pesticides (OCP)
OT  - Pyrethroid pesticides (PP)
EDAT- 2014/07/26 06:00
MHDA- 2015/05/12 06:00
CRDT- 2014/07/26 06:00
PHST- 2013/11/08 00:00 [received]
PHST- 2014/02/23 00:00 [revised]
PHST- 2014/03/03 00:00 [accepted]
PHST- 2014/07/26 06:00 [entrez]
PHST- 2014/07/26 06:00 [pubmed]
PHST- 2015/05/12 06:00 [medline]
AID - S1570-0232(14)00165-2 [pii]
AID - 10.1016/j.jchromb.2014.03.003 [doi]
PST - ppublish
SO  - J Chromatogr B Analyt Technol Biomed Life Sci. 2014 Sep 15;967:1-7. doi: 
      10.1016/j.jchromb.2014.03.003. Epub 2014 Mar 12.