PMID- 25072109
OWN - NLM
STAT- MEDLINE
DCOM- 20150420
LR  - 20140823
IS  - 1944-0057 (Electronic)
IS  - 1944-0057 (Linking)
VI  - 31
IP  - 9
DP  - 2014
TI  - Determination of hexamethylenetetramine in foods by high-performance liquid 
      chromatography (HPLC).
PG  - 1489-95
LID - 10.1080/19440049.2014.942706 [doi]
AB  - A simple and rapid method was developed and validated for the determination of 
      hexamethylenetetramine (HMT) in foods. Samples were homogenised and extracted 
      with methanol, followed by centrifugation. The resulting solution was filtered 
      and injected into the high-performance liquid chromatograph (HPLC). HMT was 
      separated using a Zorbax SCX-300 column coupled to a photodiode array detector. 
      The calibration curve was linear in the range of 1.0-100 mug ml(-1), with good 
      correlation coefficients (r(2) = 0.9992). The recoveries of HMT from foods spiked 
      at levels of 10, 50 and 100 mg kg(-1) ranged from 91.6% to 103.8%, with relative 
      standard deviations (RSDs) between 0.9% and 5.3%. The limit of detection and the 
      limit of quantification of HMT were 0.3 and 1.0 mg kg(-1) based on three food 
      matrixes (provolone cheese, glass noodle and tofu snack), respectively. 
      Uncertainty associated with accuracy contributed mostly to the expanded 
      uncertainty. No detectable levels of HMT were found in any of the samples 
      retailed in Korea. The method was successful in determining HMT in foods.
FAU - Lim, HoSoo
AU  - Lim H
AD  - a Food Additives and Packages Division , Ministry of Food and Drug Safety , 
      Chungcheongbuk-do , Korea.
FAU - Kim, JungIm
AU  - Kim J
FAU - Ko, KyungYuk
AU  - Ko K
FAU - Kim, Meehye
AU  - Kim M
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20140729
PL  - England
TA  - Food Addit Contam Part A Chem Anal Control Expo Risk Assess
JT  - Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & 
      risk assessment
JID - 101485040
RN  - 0 (Solvents)
RN  - J50OIX95QV (Methenamine)
SB  - IM
MH  - Chromatography, Liquid/*methods
MH  - Food Analysis/*methods
MH  - Methenamine/*chemistry
MH  - Reproducibility of Results
MH  - Sensitivity and Specificity
MH  - Solvents
MH  - Uncertainty
OTO - NOTNLM
OT  - hexamethylenetetramine
OT  - high-performance liquid chromatography
EDAT- 2014/07/30 06:00
MHDA- 2015/04/22 06:00
CRDT- 2014/07/30 06:00
PHST- 2014/07/30 06:00 [entrez]
PHST- 2014/07/30 06:00 [pubmed]
PHST- 2015/04/22 06:00 [medline]
AID - 10.1080/19440049.2014.942706 [doi]
PST - ppublish
SO  - Food Addit Contam Part A Chem Anal Control Expo Risk Assess. 2014;31(9):1489-95. 
      doi: 10.1080/19440049.2014.942706. Epub 2014 Jul 29.