PMID- 25269268
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20150901
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 32
IP  - 6
DP  - 2014 Jun
TI  - [Determination of three ester compounds in gasoline by two-dimensional gas 
      chromatography].
PG  - 662-5
AB  - A simple and efficient method based on the technique of packed column 
      switching-back flushing was established for the analysis of the ester compounds 
      (including ethyl acetate, sec-butyl acetate, dimethyl carbonate) in gasoline. 
      With the use of a non-polar pre-column, we successfully separated the components 
      in gasoline by back flushing out components heavier than n-octane, while the 
      lighter components and the ester compounds were flushed into a polar analytical 
      column. In this method, external standard method was applied for quantification. 
      As a result, good linear relationships existed among the three ester compounds in 
      the range of 50 mg/L to 50 000 mg/L. The linear correlation coefficients (r2) for 
      ethyl acetate, sec-butyl acetate and dimethyl carbonate were 0.999 99, 1.000 00 
      and 0.999 95, respectively. The relative standard deviations (RSDs) of standard 
      samples in six continuous tests were within 1.0%. The recoveries were between 
      98.7% and 107.9%. The detection limit of the method (S/N = 3) was 5 mg/L. No 
      pretreatment was needed. This method is simple, accurate, quick as well as 
      efficient, and can be used as an ideal method for the analysis of the ester 
      compounds in gasoline.
FAU - Zhao, Yan
AU  - Zhao Y
FAU - Xu, Dongyu
AU  - Xu D
FAU - Lin, Haoxue
AU  - Lin H
FAU - Chen, Xiaoyan
AU  - Chen X
FAU - Chen, Zeyong
AU  - Chen Z
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2014/10/02 06:00
MHDA- 2014/10/02 06:01
CRDT- 2014/10/02 06:00
PHST- 2014/10/02 06:00 [entrez]
PHST- 2014/10/02 06:00 [pubmed]
PHST- 2014/10/02 06:01 [medline]
AID - 10.3724/sp.j.1123.2014.01045 [doi]
PST - ppublish
SO  - Se Pu. 2014 Jun;32(6):662-5. doi: 10.3724/sp.j.1123.2014.01045.