PMID- 25434128
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20150901
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 32
IP  - 8
DP  - 2014 Aug
TI  - [Determination of residual glycol ethers in leather and leather products by gas 
      chromatography/mass spectrometry].
PG  - 890-6
AB  - An effective method was established for the simultaneous determination of 
      residual glycol ethers in leather and leather products by gas chromatography/mass 
      spectrometry. Glycol ethers in leather and leather products were ultrasonically 
      extracted at 45  degrees C, using ethyl acetate as the extraction solvent. The extracts 
      were purified by solid phase extraction (SPE) columns, and then analyzed by gas 
      chromatography/mass spectrometry in selected ion monitoring mode. The content of 
      each analyte was calibrated by external standard method. The limit of detection 
      of ethylene glycol ethyl ether (EGEE) was 0. 10 mg/kg under the condition of 
      signal to noise (S/N) of 3 and the limits of the other 11 glycol ethers were all 
      less than 0.05 mg/kg. The spiked recoveries varied from 81. 2% to 95. 5% at three 
      different spiked levels with the relative standard deviations (RSDs) ranged from 
      1.4% to 6. 6%. The proposed method is simple, rapid and accurate, with the limits 
      of detection much less than the requirements of the Regulation Concerning 
      Registration, Evaluation, Authorization and Restriction of Chemicals (REACH) of 
      European Union. It is applicable to the determination of residual glycol ethers 
      in leather and leather products, and provides a reference for the relevant 
      testing standards.
FAU - Wang, Ghengyun
AU  - Wang G
FAU - Zhang, Weiya
AU  - Zhang W
FAU - Li, Lixia
AU  - Li L
FAU - Shen, Yalei
AU  - Shen Y
FAU - Lin, Junfeng
AU  - Lin J
FAU - Xie, Tangtang
AU  - Xie T
FAU - Chu, Naiqing
AU  - Chu N
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2014/12/02 06:00
MHDA- 2014/12/02 06:01
CRDT- 2014/12/02 06:00
PHST- 2014/12/02 06:00 [entrez]
PHST- 2014/12/02 06:00 [pubmed]
PHST- 2014/12/02 06:01 [medline]
AID - 10.3724/sp.j.1123.2014.04008 [doi]
PST - ppublish
SO  - Se Pu. 2014 Aug;32(8):890-6. doi: 10.3724/sp.j.1123.2014.04008.