PMID- 25597092
OWN - NLM
STAT- MEDLINE
DCOM- 20150726
LR  - 20181202
IS  - 1671-7104 (Print)
IS  - 1671-7104 (Linking)
VI  - 38
IP  - 5
DP  - 2014 Sep
TI  - [Determination of residual cyclohexanone in disposable infusion set by gas 
      chromatography].
PG  - 381-2, 385
AB  - An effective GC method was established for contents determination of the residual 
      solvent of cyclohexanone in infusion sets for single use. The cyclohexanone in 
      infusion sets for single use products were extracted with circular pump, using 
      ethylalcohol as the extraction solven, then the extract followed by analysis of 
      gas chromatography-tandem mass spectrometry. The method was simple, rapid, 
      sensitive and accurate, Cyclohexanone showed good linearity in the range of 
      (5.5-190.9) mug/mL, the correlation coefficient was 0.999 0, the detection limit 
      (S/N = 3) was 0.133 mug/mL and limits of quantitation (S/N = 10) was 1.33 mug/mL. 
      The spiked average recoveries ranged from 98% to 99%. The relative standard 
      deviations (RSDs) of the method ranged from 1.03% to 1.98%. The method was 
      simple, fast, sensitive and accurate, and may serve as a mass control method for 
      residual cyclohexanone in disposable infusion sets for single use.
FAU - Zhang, Li
AU  - Zhang L
AD  - Medical Device Supervising and Testing Center of Hangzhou, State Food and Drug 
      Administration, Hangzhou. fancyzl11@163.com
FAU - Wen, Yan
AU  - Wen Y
FAU - He, Tao
AU  - He T
FAU - Wang, Minzhu
AU  - Wang M
FAU - Xu, Pinghua
AU  - Xu P
LA  - chi
PT  - Journal Article
PL  - China
TA  - Zhongguo Yi Liao Qi Xie Za Zhi
JT  - Zhongguo yi liao qi xie za zhi = Chinese journal of medical instrumentation
JID - 9426153
RN  - 0 (Cyclohexanones)
RN  - 0 (Solvents)
RN  - 5QOR3YM052 (cyclohexanone)
SB  - IM
MH  - Cyclohexanones/*analysis
MH  - Disposable Equipment/*standards
MH  - Gas Chromatography-Mass Spectrometry
MH  - Solvents/analysis
EDAT- 2015/01/20 06:00
MHDA- 2015/07/28 06:00
CRDT- 2015/01/20 06:00
PHST- 2015/01/20 06:00 [entrez]
PHST- 2015/01/20 06:00 [pubmed]
PHST- 2015/07/28 06:00 [medline]
PST - ppublish
SO  - Zhongguo Yi Liao Qi Xie Za Zhi. 2014 Sep;38(5):381-2, 385.