PMID- 25764658
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20150901
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 32
IP  - 11
DP  - 2014 Nov
TI  - [Rapid detection of eight fluorescent whitening agents in textile by ultra 
      performance convergence chromatography].
PG  - 1230-5
AB  - An accurate quantitative and confirmative method has been developed for the 
      deter- mination of eight fluorescent whitening agents (FWAs) in textile by ultra 
      performance conver- gence chromatography (UPC2) coupled with photo diode array 
      (PDA) detection, including 1,2-bis (5-methyl-2-benzoxazole) ethylene (PF), 
      7-diethylamino-4-methylcoumarin (SWN), 2, 2'-(2,5-thiophenediyl) 
      bis(5-(1,1-dimethylethyl)-benzoxazol (OB), 2-[4-[2-[4-(2-benzox- azolyl) phenyl] 
      ethenyl] phenyl] -5-methyl-benzoxazol (KSN), 1,4-bis (2-cyanostyryl) benzene 
      (ER-I), 1-(2-cyanostyryl)-4-(4-cyanostyryl) benzene (ER-II), 
      2,2'-(1,4-naphthalenediyl) bis-benzoxazol (KCB), 4,4'-bis[2-(2-methoxyphenyl) 
      ethenyl]-1,1'-biphenyl (FP). The sample was extracted with xylene and 
      concentrated by a rotary evaporator, and then qualitatively and quantitatively 
      analyzed by UPC2. The separation of target compounds was achieved on an ACQUITY 
      UPC2 HSS C18 SB column (100 mm x 3.0 mm, 1.8 mum) by a gradient elution with 
      supercritical carbon dioxide and methanol as mobile phases. External standard 
      method was used for the quantitative determination and the calibration curves 
      showed good linearity in the concentration range of 1.0-20.0 mg/L for the eight 
      target compounds with correlation coefficients not less than 0.999 1. The limits 
      of quantification of the eight compounds (LOQs, S/N = 10) were 0.70-0.95 mg/L. 
      The average recoveries of the eight compounds ranged from 90.9% to 96.5% at the 
      spiked levels of 2.0, 5.0, 10.0 mg/kg with the relative standard deviations 
      (RSDs) of 2.8%-4.2%. The method is simple, accurate and time-saving with high 
      sensitivity, and can be used for the rapid determination of the eight FWAs in 
      textile.
FAU - Tang, Juan
AU  - Tang J
FAU - Ding, Youchao
AU  - Ding Y
FAU - Cao, Xizhong
AU  - Cao X
FAU - Qi, Yan
AU  - Qi Y
FAU - Qian, Kai
AU  - Qian K
LA  - chi
PT  - English Abstract
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
EDAT- 2015/03/15 06:00
MHDA- 2015/03/15 06:01
CRDT- 2015/03/14 06:00
PHST- 2015/03/14 06:00 [entrez]
PHST- 2015/03/15 06:00 [pubmed]
PHST- 2015/03/15 06:01 [medline]
AID - 10.3724/sp.j.1123.2014.07030 [doi]
PST - ppublish
SO  - Se Pu. 2014 Nov;32(11):1230-5. doi: 10.3724/sp.j.1123.2014.07030.