PMID- 25971112 OWN - NLM STAT- PubMed-not-MEDLINE DCOM- 20150612 LR - 20190715 IS - 1533-4899 (Electronic) IS - 1533-4880 (Linking) VI - 14 IP - 12 DP - 2014 Dec TI - Surface nanocrystallization of pure Cu induced by ultrasonic shot peening. PG - 9637-43 AB - Peening is mainly used as a method of surface treatment for microstructural modification in order to improve surface mechanical properties. The ultrasonic shot peening (USP) technique can cause severe plastic deformation with its high strain rate on the surface of metallic parts. However, systematic studies of microstructural refinement mechanism upon plastic deformation with consideration of alloy systems are rare. In this study, USP-treated Cu samples of 99.96% purity was examined using analytical techniques, Vickers microhardness test, electron backscattered diffraction (EBSD) and transmission electron microscopy (TEM). Results of EBSD and microhardness analyses indicated grain refinement with deformation structures and hardness increase down to 400 mum in depth upon treatment. Depth specific TEM analysis of the samples revealed the steps of the grain refinement process to the formation of randomly oriented fine grains. FAU - Li, Kejian AU - Li K FAU - He, Yinsheng AU - He Y FAU - Fang, Chao AU - Fang C FAU - Ma, Houyu AU - Ma H FAU - Kim, Jaeyong AU - Kim J FAU - Lee, Han-Sang AU - Lee HS FAU - Song, Jung-Il AU - Song JI FAU - Yang, Cheol-Woong AU - Yang CW FAU - Lee, Je-Hyun AU - Lee JH FAU - Shin, Keesam AU - Shin K LA - eng PT - Journal Article PT - Research Support, Non-U.S. Gov't PL - United States TA - J Nanosci Nanotechnol JT - Journal of nanoscience and nanotechnology JID - 101088195 EDAT- 2015/05/15 06:00 MHDA- 2015/05/15 06:01 CRDT- 2015/05/15 06:00 PHST- 2015/05/15 06:00 [entrez] PHST- 2015/05/15 06:00 [pubmed] PHST- 2015/05/15 06:01 [medline] AID - 10.1166/jnn.2014.10176 [doi] PST - ppublish SO - J Nanosci Nanotechnol. 2014 Dec;14(12):9637-43. doi: 10.1166/jnn.2014.10176.