PMID- 26003698
OWN - NLM
STAT- MEDLINE
DCOM- 20160219
LR  - 20150525
IS  - 1873-3573 (Electronic)
IS  - 0039-9140 (Linking)
VI  - 142
DP  - 2015 Sep 1
TI  - Use of ZIF-8-derived nanoporous carbon as the adsorbent for the solid phase 
      extraction of carbamate pesticides prior to high-performance liquid 
      chromatographic analysis.
PG  - 104-9
LID - S0039-9140(15)00272-6 [pii]
LID - 10.1016/j.talanta.2015.04.034 [doi]
AB  - In this work, a chemically and thermally robust and highly porous zeolite-type 
      metal-organic framework, zeolitic imidazolate framework-8 (ZIF-8), was used as 
      both a precursor and a template and furfuryl alcohol as a second precursor to 
      synthesize a nanoporous carbon. The prepared ZIF-8-derived nanoporous carbon was 
      used as the solid-phase extraction adsorbent for the extraction of carbamate 
      pesticides from cabbage and water samples. The adsorbed analytes were eluted with 
      acetonitrile for the determination by high performance liquid 
      chromatography-ultraviolet detection. The high surface area, high porosity, good 
      stability and fast adsorption/desorption kinetics of the material enabled it to 
      have a high adsorption capacity and good adsorption performance. Under optimum 
      conditions, good linearity for the analytes in the range of 0.5-100 ng g(-1) and 
      0.05-20 ng mL(-1) existed for cabbage and water samples with the correlation 
      coefficients of 0.9968-0.9980 and 0.9990-0.9995, respectively. The limits of 
      detection (S/N=3) for the analytes were in the range of 0.25-0.1 ng g(-1) and 
      0.01-0.02 ng mL(-1) for the cabbage and water samples, respectively. The relative 
      standard deviations (RSDs) for intra-day and the inter-day determinations of the 
      analytes were below 7.0% and 12.5%, respectively.
CI  - Copyright (c) 2015 Elsevier B.V. All rights reserved.
FAU - Hao, Lin
AU  - Hao L
AD  - College of Science, Agricultural University of Hebei, Baoding 071001, China.
FAU - Liu, Xingli
AU  - Liu X
AD  - College of Science, Agricultural University of Hebei, Baoding 071001, China.
FAU - Wang, Juntao
AU  - Wang J
AD  - College of Science, Agricultural University of Hebei, Baoding 071001, China.
FAU - Wang, Chun
AU  - Wang C
AD  - College of Science, Agricultural University of Hebei, Baoding 071001, China.
FAU - Wu, Qiuhua
AU  - Wu Q
AD  - College of Science, Agricultural University of Hebei, Baoding 071001, China.
FAU - Wang, Zhi
AU  - Wang Z
AD  - College of Science, Agricultural University of Hebei, Baoding 071001, China. 
      Electronic address: zhiwang2013@aliyun.com.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20150422
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
RN  - 0 (Carbamates)
RN  - 0 (Drinking Water)
RN  - 0 (Imidazoles)
RN  - 0 (Organometallic Compounds)
RN  - 0 (Pesticides)
RN  - 0 (Water Pollutants, Chemical)
RN  - 1318-02-1 (Zeolites)
RN  - 7440-44-0 (Carbon)
RN  - J41CSQ7QDS (Zinc)
SB  - IM
MH  - Adsorption
MH  - Brassica/chemistry
MH  - Carbamates/*analysis/chemistry
MH  - Carbon/*chemistry
MH  - Chromatography, High Pressure Liquid
MH  - Drinking Water/analysis
MH  - Imidazoles/*chemistry
MH  - Nanostructures/chemistry
MH  - Organometallic Compounds/*chemistry
MH  - Pesticides/*analysis/chemistry
MH  - Porosity
MH  - Solid Phase Extraction
MH  - Water Pollutants, Chemical/analysis/chemistry
MH  - Zeolites/*chemistry
MH  - Zinc/*chemistry
OTO - NOTNLM
OT  - Carbamate pesticides
OT  - High performance liquid chromatography
OT  - Solid phase extraction
OT  - Zeolitic imidazolate framework-8-derived nanoporous carbon
EDAT- 2015/05/25 06:00
MHDA- 2016/02/20 06:00
CRDT- 2015/05/25 06:00
PHST- 2015/01/06 00:00 [received]
PHST- 2015/04/07 00:00 [revised]
PHST- 2015/04/12 00:00 [accepted]
PHST- 2015/05/25 06:00 [entrez]
PHST- 2015/05/25 06:00 [pubmed]
PHST- 2016/02/20 06:00 [medline]
AID - S0039-9140(15)00272-6 [pii]
AID - 10.1016/j.talanta.2015.04.034 [doi]
PST - ppublish
SO  - Talanta. 2015 Sep 1;142:104-9. doi: 10.1016/j.talanta.2015.04.034. Epub 2015 Apr 
      22.