PMID- 26125614
OWN - NLM
STAT- MEDLINE
DCOM- 20160428
LR  - 20150729
IS  - 1944-0057 (Electronic)
IS  - 1944-0057 (Linking)
VI  - 32
IP  - 8
DP  - 2015
TI  - High-throughput determination of citrinin in rice by ultra-high-performance 
      liquid chromatography and fluorescence detection (UHPLC-FL).
PG  - 1352-7
LID - 10.1080/19440049.2015.1055522 [doi]
AB  - A rapid, simple and effective method for the determination of citrinin in rice by 
      UHPLC coupled to fluorescence detection has been developed and validated. 
      Extraction of citrinin from rice samples was achieved by applying a 
      QuEChERS-based extraction/partitioning process with water and acetonitrile, 
      without the need of further extract clean-up. The method was fully validated for 
      white rice, and its applicability in other rice matrices, such as brown and red 
      rice, was confirmed by recovery experiments. Under optimum conditions, recoveries 
      ranged from 72.5% to 92.8%, with relative standard deviations (RSDs) lower than 
      7.1%. Detection and quantification limits were estimated to be 1.5 and 
      5.0 microg kg(-1), respectively. Finally, 21 organic rice samples were analysed, but 
      none was contaminated with citrinin above the detection limit of the method. The 
      method proved to be fast and non-laborious.
FAU - Huertas-Perez, Jose F
AU  - Huertas-Perez JF
AD  - a Department of Analytical Chemistry, Faculty of Sciences , University of Granada 
      , Granada , Spain.
FAU - Arroyo-Manzanares, Natalia
AU  - Arroyo-Manzanares N
FAU - Garcia-Campana, Ana M
AU  - Garcia-Campana AM
FAU - Gamiz-Gracia, Laura
AU  - Gamiz-Gracia L
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20150630
PL  - England
TA  - Food Addit Contam Part A Chem Anal Control Expo Risk Assess
JT  - Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & 
      risk assessment
JID - 101485040
RN  - 3S697X6SNZ (Citrinin)
SB  - IM
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Citrinin/*analysis
MH  - Fluorescence
MH  - Food Contamination/*analysis
MH  - Limit of Detection
MH  - Oryza/*chemistry
MH  - Reproducibility of Results
OTO - NOTNLM
OT  - QuEChERS
OT  - UHPLC
OT  - citrinin
OT  - rice
OT  - sample preparation
EDAT- 2015/07/01 06:00
MHDA- 2016/04/29 06:00
CRDT- 2015/07/01 06:00
PHST- 2015/07/01 06:00 [entrez]
PHST- 2015/07/01 06:00 [pubmed]
PHST- 2016/04/29 06:00 [medline]
AID - 10.1080/19440049.2015.1055522 [doi]
PST - ppublish
SO  - Food Addit Contam Part A Chem Anal Control Expo Risk Assess. 2015;32(8):1352-7. 
      doi: 10.1080/19440049.2015.1055522. Epub 2015 Jun 30.