PMID- 26182466
OWN - NLM
STAT- MEDLINE
DCOM- 20150901
LR  - 20190923
IS  - 1000-8713 (Print)
IS  - 1000-8713 (Linking)
VI  - 33
IP  - 3
DP  - 2015 Mar
TI  - [Determination of four frequently-used essences in foods by ultra performance 
      liquid chromatography-tandem mass spectrometry].
PG  - 250-5
AB  - A method has been developed for the simultaneous determination of vanillin, ethyl 
      vanillin, maltol and ethyl maltol in foods by ultra performance liquid 
      chromatography coupled with electrospray ionization tandem mass spectrometry 
      (UPLC-ESI-MS/MS). The sample was extracted with ultrapure water, and purified 
      with SPE column. The target compounds were separated on a C18 column with the 
      gradient elution of methanol and water containing 0.002 mol/L ammonium acetate 
      and 0.1% (v/v) formic acid. The four components were determined in the modes of 
      electrospray positive ionization (ESI+) and multiple reaction monitoring (MRM). 
      The linear ranges were 10-1,000 microg/L for vanillin and maltol and 5-500 microg/L for 
      ethyl vanillin and ethyl maltol, with the correlation coefficients more than 
      0.999. The recoveries of the four compounds ranged from 75.8% to 116%, with the 
      relative standard deviations (RSDs) of 1.58%-4.01%. The method showed good 
      extraction efficiency, high sensitivity and good reproducibility. It is suitable 
      for the simultaneous detection of vanillin, ethyl vanillin, maltol and ethyl 
      maltol in foods.
FAU - Yang, Huamei
AU  - Yang H
FAU - Hang, Li
AU  - Hang L
LA  - chi
PT  - Journal Article
PL  - China
TA  - Se Pu
JT  - Se pu = Chinese journal of chromatography
JID - 9424804
RN  - 0 (Flavoring Agents)
SB  - IM
MH  - *Chromatography, High Pressure Liquid
MH  - Flavoring Agents/*analysis
MH  - Food Analysis/*methods
MH  - Reproducibility of Results
MH  - Spectrometry, Mass, Electrospray Ionization
MH  - *Tandem Mass Spectrometry
EDAT- 2015/07/18 06:00
MHDA- 2015/09/02 06:00
CRDT- 2015/07/18 06:00
PHST- 2015/07/18 06:00 [entrez]
PHST- 2015/07/18 06:00 [pubmed]
PHST- 2015/09/02 06:00 [medline]
AID - 10.3724/sp.j.1123.2014.11018 [doi]
PST - ppublish
SO  - Se Pu. 2015 Mar;33(3):250-5. doi: 10.3724/sp.j.1123.2014.11018.