PMID- 26218576
OWN - NLM
STAT- MEDLINE
DCOM- 20160503
LR  - 20181113
IS  - 1932-6203 (Electronic)
IS  - 1932-6203 (Linking)
VI  - 10
IP  - 7
DP  - 2015
TI  - The Rapid Screening of Triazophos Residues in Agricultural Products by 
      Chemiluminescent Enzyme Immunoassay.
PG  - e0133839
LID - 10.1371/journal.pone.0133839 [doi]
LID - e0133839
AB  - A highly sensitive chemiluminescent enzyme immunoassay (CLEIA) method was 
      developed in this study for efficient screening of triazophos residues in a large 
      number of samples. Based on the maximum residue limits (MRLs) set by China and 
      CAC for triazophos in different agro-products, the representative apple, orange, 
      cabbage, zucchini, and rice samples were selected as spiked samples, and the 
      triazophos at the concentrations of the MRL values were spiked to blank samples. 
      Subsequently, the five samples with the spiked triazophos standard were measured 
      by CLEIA 100 times, and the detection results indicated that the correction 
      factors of the apple, orange, cabbage, zucchini, and rice were determined as 
      0.79, 0.66, 0.85, 0.76, and 0.91, respectively. In this experiment, 1500 real 
      samples were detected by both the CLEIA and the GC-MS methods. With the GC-MS 
      method, 1462 samples were identified as negative samples and 38 samples as 
      positive samples. Based on the correction factors, the false positive rate of the 
      CLEIA method was 0.13%, and false negative rate was 0. The results showed that 
      the established CLEIA method could be used to screen a large number of real 
      samples.
FAU - Chen, Ge
AU  - Chen G
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Yang, Lihua
AU  - Yang L
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Jin, Maojun
AU  - Jin M
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Du, Pengfei
AU  - Du P
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Zhang, Chan
AU  - Zhang C
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Wang, Jian
AU  - Wang J
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Shao, Hua
AU  - Shao H
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Jin, Fen
AU  - Jin F
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Zheng, Lufei
AU  - Zheng L
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Wang, Shanshan
AU  - Wang S
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - She, Yongxin
AU  - She Y
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
FAU - Wang, Jing
AU  - Wang J
AD  - Key Laboratory for Agro-Products Quality and Safety, Institute of Quality 
      Standards & Testing Technology for Agro-Products, Chinese Academy of Agricultural 
      Sciences, Beijing, 100081, China.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20150728
PL  - United States
TA  - PLoS One
JT  - PloS one
JID - 101285081
RN  - 0 (Organothiophosphates)
RN  - 0 (Triazoles)
RN  - 6099J8L0EE (triazophos)
SB  - IM
MH  - Agriculture
MH  - China
MH  - Fruit/*chemistry
MH  - Gas Chromatography-Mass Spectrometry
MH  - High-Throughput Screening Assays/*methods
MH  - Immunoenzyme Techniques/*methods
MH  - Luminescent Measurements/*methods
MH  - Organothiophosphates/*analysis
MH  - Triazoles/*analysis
MH  - Vegetables/*chemistry
PMC - PMC4517747
COIS- Competing Interests: The authors have declared that no competing interests exist.
EDAT- 2015/07/29 06:00
MHDA- 2016/05/04 06:00
PMCR- 2015/07/28
CRDT- 2015/07/29 06:00
PHST- 2015/01/19 00:00 [received]
PHST- 2015/07/02 00:00 [accepted]
PHST- 2015/07/29 06:00 [entrez]
PHST- 2015/07/29 06:00 [pubmed]
PHST- 2016/05/04 06:00 [medline]
PHST- 2015/07/28 00:00 [pmc-release]
AID - PONE-D-15-02572 [pii]
AID - 10.1371/journal.pone.0133839 [doi]
PST - epublish
SO  - PLoS One. 2015 Jul 28;10(7):e0133839. doi: 10.1371/journal.pone.0133839. 
      eCollection 2015.