PMID- 26431856
OWN - NLM
STAT- MEDLINE
DCOM- 20160322
LR  - 20231213
IS  - 1873-3778 (Electronic)
IS  - 0021-9673 (Linking)
VI  - 1418
DP  - 2015 Oct 30
TI  - Rapid and sensitive multiresidue analysis of pesticides in tobacco using low 
      pressure and traditional gas chromatography tandem mass spectrometry.
PG  - 228-232
LID - S0021-9673(15)01390-4 [pii]
LID - 10.1016/j.chroma.2015.09.070 [doi]
AB  - Public exposure to pesticide residues through the main/side-stream smoke of 
      tobacco (Nicotiana tabacum L.) is an international concern. This article reports 
      optimization and validation of large-scale multiresidue analysis methods 
      involving low pressure and traditional gas chromatography tandem mass 
      spectrometry in compliance with the guidance residue levels (GRLs) of Cooperative 
      Centre for Scientific Research Relative to Tobacco (CORESTA). Analysis by low 
      pressure GC-MS/MS offered three times rapid turn around time over the traditional 
      GC-MS/MS with limits of quantifications (LOQs) less than 2mug/L for all the 259 
      test compounds and the recoveries in the range of 70-118% (+/-20%) at 10 and 
      20mug/kg levels of fortification.
CI  - Copyright (c) 2015 Elsevier B.V. All rights reserved.
FAU - Khan, Zareen S
AU  - Khan ZS
AD  - National Referral Laboratory, ICAR-National Research Centre for Grapes, P.O. 
      Manjri Farm, Pune 412 307, India.
FAU - Girame, Rushali
AU  - Girame R
AD  - National Referral Laboratory, ICAR-National Research Centre for Grapes, P.O. 
      Manjri Farm, Pune 412 307, India.
FAU - Utture, Sagar C
AU  - Utture SC
AD  - National Referral Laboratory, ICAR-National Research Centre for Grapes, P.O. 
      Manjri Farm, Pune 412 307, India.
FAU - Ghosh, Rakesh Kumar
AU  - Ghosh RK
AD  - ICAR-Central Tobacco Research Institute, Rajahmundry, Andhra Pradesh 533 105, 
      India.
FAU - Banerjee, Kaushik
AU  - Banerjee K
AD  - National Referral Laboratory, ICAR-National Research Centre for Grapes, P.O. 
      Manjri Farm, Pune 412 307, India. Electronic address: kbgrape@yahoo.com.
LA  - eng
PT  - Journal Article
DEP - 20150926
PL  - Netherlands
TA  - J Chromatogr A
JT  - Journal of chromatography. A
JID - 9318488
RN  - 0 (Pesticide Residues)
RN  - 0 (Smoke)
SB  - IM
MH  - Gas Chromatography-Mass Spectrometry/methods
MH  - Pesticide Residues/*analysis
MH  - Smoke/*analysis
MH  - Tandem Mass Spectrometry/methods
MH  - Nicotiana/*chemistry
OTO - NOTNLM
OT  - GC-MS/MS
OT  - Low pressure GC-MS/MS
OT  - Method validation
OT  - Multiresidue analysis of pesticides in tobacco
EDAT- 2015/10/04 06:00
MHDA- 2016/03/24 06:00
CRDT- 2015/10/04 06:00
PHST- 2015/07/07 00:00 [received]
PHST- 2015/09/18 00:00 [revised]
PHST- 2015/09/22 00:00 [accepted]
PHST- 2015/10/04 06:00 [entrez]
PHST- 2015/10/04 06:00 [pubmed]
PHST- 2016/03/24 06:00 [medline]
AID - S0021-9673(15)01390-4 [pii]
AID - 10.1016/j.chroma.2015.09.070 [doi]
PST - ppublish
SO  - J Chromatogr A. 2015 Oct 30;1418:228-232. doi: 10.1016/j.chroma.2015.09.070. Epub 
      2015 Sep 26.