PMID- 26434342
OWN - NLM
STAT- MEDLINE
DCOM- 20160411
LR  - 20181202
IS  - 1873-7072 (Electronic)
IS  - 0308-8146 (Linking)
VI  - 132
IP  - 1
DP  - 2012 May 1
TI  - Analysis of six fungicides and one acaricide in still and fortified wines using 
      solid-phase microextraction-gas chromatography/tandem mass spectrometry.
PG  - 630-6
LID - S0308-8146(11)01573-1 [pii]
LID - 10.1016/j.foodchem.2011.10.102 [doi]
AB  - A multiresidue gas chromatographic method for the determination of six fungicides 
      (captan, chlorthalonil, folpet, iprodione, procymidone and vinclozolin) and one 
      acaricide (dicofol) in still and fortified wines was developed. Solid-phase 
      microextraction (SPME) was chosen for the extraction of the compounds from the 
      studied matrices and tandem mass spectrometry (MS/MS) detection was used. The 
      extraction consists in a solvent free and automated procedure and the detection 
      is highly sensitive and selective. Good linearity was obtained with correlation 
      coefficients of regression (R(2))>0.99 for all the compounds. Satisfactory 
      results of repeatability and intermediate precision were obtained for most of the 
      analytes (RSD⩽20%). Recoveries from spiked wine ranged from 80.1% to 112.0%. 
      Limits of quantification (LOQs) were considerably below the proposed maximum 
      residue limits (MRLs) for these compounds in grapes and below the suggested 
      limits for wine (MRLs/10), with the exception of captan.
CI  - Copyright (c) 2011 Elsevier Ltd. All rights reserved.
FAU - Martins, Joana
AU  - Martins J
AD  - IVDP, Instituto dos Vinhos do Douro e do Porto, Rua de Ferreira Borges, 27, 
      4050-253 Porto, Portugal; REQUIMTE, Instituto Superior de Engenharia do Porto, 
      Rua Dr. Antonio Bernardino de Almeida, 431, 4200-072 Porto, Portugal.
FAU - Esteves, Cristina
AU  - Esteves C
AD  - IVDP, Instituto dos Vinhos do Douro e do Porto, Rua de Ferreira Borges, 27, 
      4050-253 Porto, Portugal.
FAU - Limpo-Faria, Ana
AU  - Limpo-Faria A
AD  - IVDP, Instituto dos Vinhos do Douro e do Porto, Rua de Ferreira Borges, 27, 
      4050-253 Porto, Portugal.
FAU - Barros, Paulo
AU  - Barros P
AD  - IVDP, Instituto dos Vinhos do Douro e do Porto, Rua de Ferreira Borges, 27, 
      4050-253 Porto, Portugal.
FAU - Ribeiro, Natalia
AU  - Ribeiro N
AD  - IVDP, Instituto dos Vinhos do Douro e do Porto, Rua de Ferreira Borges, 27, 
      4050-253 Porto, Portugal.
FAU - Simoes, Tomas
AU  - Simoes T
AD  - IVDP, Instituto dos Vinhos do Douro e do Porto, Rua de Ferreira Borges, 27, 
      4050-253 Porto, Portugal.
FAU - Correia, Manuela
AU  - Correia M
AD  - REQUIMTE, Instituto Superior de Engenharia do Porto, Rua Dr. Antonio Bernardino 
      de Almeida, 431, 4200-072 Porto, Portugal. Electronic address: mmb@isep.ipp.pt.
FAU - Delerue-Matos, Cristina
AU  - Delerue-Matos C
AD  - REQUIMTE, Instituto Superior de Engenharia do Porto, Rua Dr. Antonio Bernardino 
      de Almeida, 431, 4200-072 Porto, Portugal.
LA  - eng
PT  - Journal Article
DEP - 20111107
PL  - England
TA  - Food Chem
JT  - Food chemistry
JID - 7702639
RN  - 0 (Acaricides)
RN  - 0 (Fungicides, Industrial)
SB  - IM
MH  - Acaricides/analysis/*chemistry
MH  - Fungicides, Industrial/analysis/*chemistry
MH  - Gas Chromatography-Mass Spectrometry/*methods
MH  - Solid Phase Microextraction/*methods
MH  - Tandem Mass Spectrometry/*methods
MH  - Wine/*analysis
OTO - NOTNLM
OT  - Acaricide
OT  - Fungicide
OT  - GC-MS/MS
OT  - SPME
OT  - Wine
EDAT- 2012/05/01 00:00
MHDA- 2016/04/12 06:00
CRDT- 2015/10/06 06:00
PHST- 2010/07/28 00:00 [received]
PHST- 2011/08/03 00:00 [revised]
PHST- 2011/10/29 00:00 [accepted]
PHST- 2015/10/06 06:00 [entrez]
PHST- 2012/05/01 00:00 [pubmed]
PHST- 2016/04/12 06:00 [medline]
AID - S0308-8146(11)01573-1 [pii]
AID - 10.1016/j.foodchem.2011.10.102 [doi]
PST - ppublish
SO  - Food Chem. 2012 May 1;132(1):630-6. doi: 10.1016/j.foodchem.2011.10.102. Epub 
      2011 Nov 7.