PMID- 26452921
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20160728
LR  - 20151010
IS  - 1873-3573 (Electronic)
IS  - 0039-9140 (Linking)
VI  - 144
DP  - 2015 Nov 1
TI  - Simultaneous determination of three alternative flame retardants (dechlorane 
      plus, 1,2-bis(2,4,6-tribromophenoxy) ethane, and decabromodiphenyl ethane) in 
      soils by gas chromatography-high resolution mass spectrometry.
PG  - 1014-20
LID - S0039-9140(15)30161-2 [pii]
LID - 10.1016/j.talanta.2015.07.031 [doi]
AB  - A gas chromatography-high resolution mass spectrometry (GC-HRMS) method has been 
      developed for the simultaneous determination of three alternative flame 
      retardants, dechlorane plus (DP), 1,2-bis(2,4,6-tribromophenoxy) ethane (BTBPE), 
      and decabromodiphenyl ethane (DBDPE) in soils. The soil samples were extracted by 
      accelerated solvent extraction, followed by purification with concentrated 
      sulfuric acid partitioning combined with acid-base silica gel column separation. 
      The gas chromatography featured with a thermostable capillary column of short 
      length and a thin stationary phase was operated in pulse injection mode. A 
      double-focusing magnetic sector high resolution mass spectrometer with electron 
      impact ionization was used for quantification of the analytes. The method 
      detection limits were 0.27-0.33 pg for DPs, 0.41 pg for BTBPE, and 36 pg for 
      DBDPE. The mean recoveries for DPs, BTBPE, and DBDPE in spiked soils were 
      88-107%, 78-97%, and 74-113%, respectively, with relative standard deviations 
      ranging from 5.2% to 18%. The recoveries of (13)C-labeled standards for DPs, 
      BTBPE, and DBDPE in soil samples were 45-110%, 67-118%, and 27-82%, respectively. 
      These results met the acceptable range of labeled standards for analysis of 
      polybrominated diphenyl ethers as specified by the USEPA 1614 method.
CI  - Copyright (c) 2015. Published by Elsevier B.V.
FAU - Xu, Pengjun
AU  - Xu P
AD  - Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan 
      Road, Shahekou District, Dalian 116023, China; National Research Center for 
      Environmental Analysis and Measurement, 1 South Yuhui Road, Chaoyang District, 
      Beijing 100029, China; Dalian University of Technology, 2 Linggong Road, 
      Ganjingzi District, Dalian 116024, China.
FAU - Tao, Bu
AU  - Tao B
AD  - Hebei Agricultural University, 289 Lingyusi Street, Baoding 071001, China.
FAU - Ye, Zhiqiang
AU  - Ye Z
AD  - Dalian University of Technology, 2 Linggong Road, Ganjingzi District, Dalian 
      116024, China.
FAU - Qi, Li
AU  - Qi L
AD  - National Research Center for Environmental Analysis and Measurement, 1 South 
      Yuhui Road, Chaoyang District, Beijing 100029, China.
FAU - Ren, Yue
AU  - Ren Y
AD  - National Research Center for Environmental Analysis and Measurement, 1 South 
      Yuhui Road, Chaoyang District, Beijing 100029, China.
FAU - Zhou, Zhiguang
AU  - Zhou Z
AD  - National Research Center for Environmental Analysis and Measurement, 1 South 
      Yuhui Road, Chaoyang District, Beijing 100029, China.
FAU - Li, Nan
AU  - Li N
AD  - National Research Center for Environmental Analysis and Measurement, 1 South 
      Yuhui Road, Chaoyang District, Beijing 100029, China.
FAU - Huang, Yeru
AU  - Huang Y
AD  - National Research Center for Environmental Analysis and Measurement, 1 South 
      Yuhui Road, Chaoyang District, Beijing 100029, China.
FAU - Chen, Jiping
AU  - Chen J
AD  - Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan 
      Road, Shahekou District, Dalian 116023, China. Electronic address: 
      chenjp@dicp.ac.cn.
LA  - eng
PT  - Journal Article
DEP - 20150711
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
OTO - NOTNLM
OT  - 1,2-bis(2,4,6-tribromophenoxy) ethane
OT  - Alternative flame retardant
OT  - Decabromodiphenyl ethane
OT  - Dechlorane plus
OT  - Gas chromatography-high resolution mass spectrometry
OT  - Soil
EDAT- 2015/10/11 06:00
MHDA- 2015/10/11 06:01
CRDT- 2015/10/11 06:00
PHST- 2015/06/03 00:00 [received]
PHST- 2015/07/06 00:00 [revised]
PHST- 2015/07/10 00:00 [accepted]
PHST- 2015/10/11 06:00 [entrez]
PHST- 2015/10/11 06:00 [pubmed]
PHST- 2015/10/11 06:01 [medline]
AID - S0039-9140(15)30161-2 [pii]
AID - 10.1016/j.talanta.2015.07.031 [doi]
PST - ppublish
SO  - Talanta. 2015 Nov 1;144:1014-20. doi: 10.1016/j.talanta.2015.07.031. Epub 2015 
      Jul 11.