PMID- 26652314
OWN - NLM
STAT- MEDLINE
DCOM- 20160811
LR  - 20191210
IS  - 1520-5118 (Electronic)
IS  - 0021-8561 (Linking)
VI  - 64
IP  - 1
DP  - 2016 Jan 13
TI  - Nickel Oxide Nanoparticle-Deposited Silica Composite Solid-Phase Extraction for 
      Benzimidazole Residue Analysis in Milk and Eggs by Liquid Chromatography-Mass 
      Spectrometry.
PG  - 356-63
LID - 10.1021/acs.jafc.5b04672 [doi]
AB  - A novel nickel oxide nanoparticle-deposited silica (SiO2@NiO) composite was 
      prepared via liquid-phase deposition (LPD) and then employed as a solid-phase 
      extraction (SPE) sorbent. When the SPE was coupled with liquid 
      chromatography-electrospray ionization mass spectrometry (LC-ESI/MS) analysis, an 
      analytical platform for the sensitive determination of benzimidazole residues in 
      egg and milk was established. The limits of detection of nine benzimidazoles were 
      in the range of 0.8-2.2 ng/mL in milk and 0.3-2.1 ng/g in eggs, respectively, 
      which was 5-10 times superior to the methods with other adsorbents for SPE. The 
      recoveries of nine benzimidazoles spiked in milk and egg ranged from 70.8 to 
      118.7%, with relative standard deviations (RSDs) being less than 18.9%. This work 
      presented the excellent extraction performance of NiO on benzimidazoles for the 
      first time, and the applicability of the LPD technique used as sorbents for trace 
      analysis in complex matrices was also demonstrated.
FAU - Sun, Huan
AU  - Sun H
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University , Wuhan, Hubei 430072, 
      People's Republic of China.
FAU - Yu, Qiong-Wei
AU  - Yu QW
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University , Wuhan, Hubei 430072, 
      People's Republic of China.
FAU - He, Hai-Bo
AU  - He HB
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University , Wuhan, Hubei 430072, 
      People's Republic of China.
AD  - Department of Chemistry, Shanghai University , Shanghai 200444, People's Republic 
      of China.
FAU - Lu, Qian
AU  - Lu Q
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University , Wuhan, Hubei 430072, 
      People's Republic of China.
FAU - Shi, Zhi-Guo
AU  - Shi ZG
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University , Wuhan, Hubei 430072, 
      People's Republic of China.
FAU - Feng, Yu-Qi
AU  - Feng YQ
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University , Wuhan, Hubei 430072, 
      People's Republic of China.
LA  - eng
PT  - Evaluation Study
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20151222
PL  - United States
TA  - J Agric Food Chem
JT  - Journal of agricultural and food chemistry
JID - 0374755
RN  - 0 (Anthelmintics)
RN  - 0 (Benzimidazoles)
RN  - 7631-86-9 (Silicon Dioxide)
RN  - 7OV03QG267 (Nickel)
RN  - C3574QBZ3Y (nickel monoxide)
RN  - E24GX49LD8 (benzimidazole)
SB  - IM
MH  - Animals
MH  - Anthelmintics/chemistry/*isolation & purification
MH  - Benzimidazoles/chemistry/*isolation & purification
MH  - Cattle
MH  - Chickens
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Drug Residues/chemistry/*isolation & purification
MH  - Eggs/*analysis
MH  - Food Contamination/analysis
MH  - Milk/*chemistry
MH  - Nanoparticles/chemistry
MH  - Nickel/chemistry
MH  - Silicon Dioxide/chemistry
MH  - Solid Phase Extraction/instrumentation/*methods
MH  - Tandem Mass Spectrometry/*methods
OTO - NOTNLM
OT  - NiO nanoparticle
OT  - adsorbent
OT  - benzimidazoles
OT  - liquid-phase deposition
OT  - milk and egg
OT  - solid-phase extraction
EDAT- 2015/12/15 06:00
MHDA- 2016/08/12 06:00
CRDT- 2015/12/15 06:00
PHST- 2015/12/15 06:00 [entrez]
PHST- 2015/12/15 06:00 [pubmed]
PHST- 2016/08/12 06:00 [medline]
AID - 10.1021/acs.jafc.5b04672 [doi]
PST - ppublish
SO  - J Agric Food Chem. 2016 Jan 13;64(1):356-63. doi: 10.1021/acs.jafc.5b04672. Epub 
      2015 Dec 22.