PMID- 26653422
OWN - NLM
STAT- MEDLINE
DCOM- 20160920
LR  - 20161126
IS  - 1873-3573 (Electronic)
IS  - 0039-9140 (Linking)
VI  - 148
DP  - 2016
TI  - Facile synthesis of magnetic carbon nitride nanosheets and its application in 
      magnetic solid phase extraction for polycyclic aromatic hydrocarbons in edible 
      oil samples.
PG  - 46-53
LID - S0039-9140(15)30425-2 [pii]
LID - 10.1016/j.talanta.2015.10.059 [doi]
AB  - In this study, we proposed a method to fabricate magnetic carbon nitride (CN) 
      nanosheets by simple physical blending. Low-cost CN nanosheets prepared by urea 
      possessed a highly pi-conjugated structure; therefore the obtained composites were 
      employed as magnetic solid-phase extraction (MSPE) sorbent for extraction of 
      polycyclic aromatic hydrocarbons (PAHs) in edible oil samples. Moreover, sample 
      pre-treatment time could be carried out within 10 min. Thus, a simple and cheap 
      method for the analysis of PAHs in edible oil samples was established by coupling 
      magnetic CN nanosheets-based MSPE with gas chromatography-mass spectrometry 
      (GC/MS) analysis. Limits of quantitation (LOQs) for eight PAHs ranged from 0.4 to 
      0.9 ng/g. The intra- and inter-day relative standard deviations (RSDs) were less 
      than 15.0%. The recoveries of PAHs for spiked soybean oil samples ranged from 
      91.0% to 124.1%, with RSDs of less than 10.2%. Taken together, the proposed 
      method offers a simple and cost-effective option for the convenient analysis of 
      PAHs in oil samples.
CI  - Copyright (c) 2015 Elsevier B.V. All rights reserved.
FAU - Zheng, Hao-Bo
AU  - Zheng HB
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University, Wuhan 430072, China.
FAU - Ding, Jun
AU  - Ding J
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University, Wuhan 430072, China.
FAU - Zheng, Shu-Jian
AU  - Zheng SJ
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University, Wuhan 430072, China.
FAU - Zhu, Gang-Tian
AU  - Zhu GT
AD  - Key Laboratory of Tectonics and Petroleum Resources (Ministry of Education), 
      China University of Geosciences, Wuhan 430074, China.
FAU - Yuan, Bi-Feng
AU  - Yuan BF
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University, Wuhan 430072, China.
FAU - Feng, Yu-Qi
AU  - Feng YQ
AD  - Key Laboratory of Analytical Chemistry for Biology and Medicine (Ministry of 
      Education), Department of Chemistry, Wuhan University, Wuhan 430072, China. 
      Electronic address: yqfeng@whu.edu.cn.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20151023
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
RN  - 0 (Nitriles)
RN  - 0 (Plant Oils)
RN  - 0 (Polycyclic Aromatic Hydrocarbons)
RN  - 534Q0F66RK (cyanogen)
SB  - IM
MH  - *Magnetic Phenomena
MH  - Nanostructures/*chemistry
MH  - Nitriles/*chemical synthesis
MH  - Plant Oils/*analysis
MH  - Polycyclic Aromatic Hydrocarbons/*analysis
MH  - Solid Phase Extraction/*methods
OTO - NOTNLM
OT  - Edible oil
OT  - Gas chromatography-mass spectrometry
OT  - Magnetic carbon nitride nanosheets
OT  - Magnetic solid-phase extraction
OT  - Polycyclic aromatic hydrocarbons
EDAT- 2015/12/15 06:00
MHDA- 2016/09/22 06:00
CRDT- 2015/12/15 06:00
PHST- 2015/08/04 00:00 [received]
PHST- 2015/10/18 00:00 [revised]
PHST- 2015/10/22 00:00 [accepted]
PHST- 2015/12/15 06:00 [entrez]
PHST- 2015/12/15 06:00 [pubmed]
PHST- 2016/09/22 06:00 [medline]
AID - S0039-9140(15)30425-2 [pii]
AID - 10.1016/j.talanta.2015.10.059 [doi]
PST - ppublish
SO  - Talanta. 2016;148:46-53. doi: 10.1016/j.talanta.2015.10.059. Epub 2015 Oct 23.