PMID- 27066690
OWN - NLM
STAT- MEDLINE
DCOM- 20160610
LR  - 20181202
IS  - 1671-7104 (Print)
IS  - 1671-7104 (Linking)
VI  - 39
IP  - 6
DP  - 2015 Nov
TI  - [Determination of Plasticizer DEHP Released from Medical Injection Equipment].
PG  - 451-3
AB  - To established an effective GC-MS /MS method for the contents determination of 
      the residual DEHP in injection equipment, and investigate the effect of the 
      pretreatment on the measurement. To simulate the clinical conditions of use, 
      under the condition of 37 degrees C balance extraction, extract liquor by 
      chloroform extraction, then the extract followed by analysis of GC-MS /MS. The 
      method was simple, rapid, sensitive and accurate. The limits of quantitation 
      (LOQ, S/N = 5) of cyclohexanone was 0.075 mug/mL, The spiked average recoveries 
      ranged from 92% to 98%. The relative standard deviations (RSDs) of the method 
      ranged from 1.01% to 1.61%, The method was simple, fast, sensitive and accurate, 
      and may serve as a mass control method for residual DEHP in injection equipment.
FAU - Zheng, Jian
AU  - Zheng J
FAU - Wang, Minzhu
AU  - Wang M
FAU - Wang Anyan
AU  - Wang Anyan
FAU - Xu, Pinghua
AU  - Xu P
FAU - Han, Yin
AU  - Han Y
FAU - Wen, Yan
AU  - Wen Y
FAU - Zhang, Li
AU  - Zhang L
LA  - chi
PT  - Journal Article
PL  - China
TA  - Zhongguo Yi Liao Qi Xie Za Zhi
JT  - Zhongguo yi liao qi xie za zhi = Chinese journal of medical instrumentation
JID - 9426153
RN  - 0 (Cyclohexanones)
RN  - 0 (Plasticizers)
RN  - 5QOR3YM052 (cyclohexanone)
RN  - C42K0PH13C (Diethylhexyl Phthalate)
SB  - IM
MH  - Cyclohexanones/chemistry
MH  - Diethylhexyl Phthalate/*chemistry
MH  - *Equipment Contamination
MH  - *Gas Chromatography-Mass Spectrometry
MH  - Injections/instrumentation
MH  - Limit of Detection
MH  - Plasticizers/*chemistry
EDAT- 2016/04/14 06:00
MHDA- 2016/06/11 06:00
CRDT- 2016/04/13 06:00
PHST- 2016/04/13 06:00 [entrez]
PHST- 2016/04/14 06:00 [pubmed]
PHST- 2016/06/11 06:00 [medline]
PST - ppublish
SO  - Zhongguo Yi Liao Qi Xie Za Zhi. 2015 Nov;39(6):451-3.