PMID- 27080878
OWN - NLM
STAT- MEDLINE
DCOM- 20161213
LR  - 20161230
IS  - 1873-7072 (Electronic)
IS  - 0308-8146 (Linking)
VI  - 207
DP  - 2016 Sep 15
TI  - Multiresidue analysis of environmental pollutants in edible vegetable oils by gas 
      chromatography-tandem mass spectrometry.
PG  - 43-50
LID - S0308-8146(16)30444-7 [pii]
LID - 10.1016/j.foodchem.2016.03.071 [doi]
AB  - A novel multiresidue determination of polycyclic aromatic hydrocarbons (PAHs), 
      phthalate esters (PAEs) and alkylphenols (APs) in edible vegetable oils was 
      developed. The samples were extracted with hexane-saturated acetonitrile, and 
      after concentration, the extract was directly qualitatively and quantitatively 
      analyzed by gas chromatography-tandem mass spectrometry (GC-MS/MS) with multiple 
      reaction monitoring (MRM) in positive ion mode. The calibration curve displayed 
      good linearity in the range of 2-100 mug/L, with correlation coefficients greater 
      than 0.99. The mean recoveries were 70.0-110.8% by analysis of spiked oil, and 
      the relative standard deviations (RSDs) were 2.1-10.2% (n=6), respectively. The 
      limits of detection (LODs) for the 23 PAHs, 17 PAEs and 3 APs were 0.1-1.0 mug/kg, 
      0.1-4.0 mug/kg and 1.2-3.0 mug/kg, respectively. The established method effectively 
      avoided interference from large amounts of lipids and pigments. It was applied to 
      real sample and shown to be a rapid and reliable alternative for determination 
      and confirmation in routine analysis.
CI  - Copyright (c) 2016 Elsevier Ltd. All rights reserved.
FAU - Zhou, Rui-Ze
AU  - Zhou RZ
AD  - Beijing Municipal Center for Food Safety Monitoring and Risk Assessment, Beijing 
      100041, People's Republic of China.
FAU - Jiang, Jie
AU  - Jiang J
AD  - Beijing Municipal Center for Food Safety Monitoring and Risk Assessment, Beijing 
      100041, People's Republic of China.
FAU - Mao, Ting
AU  - Mao T
AD  - Beijing Municipal Center for Food Safety Monitoring and Risk Assessment, Beijing 
      100041, People's Republic of China.
FAU - Zhao, Ya-Song
AU  - Zhao YS
AD  - Beijing Municipal Center for Food Safety Monitoring and Risk Assessment, Beijing 
      100041, People's Republic of China.
FAU - Lu, Yong
AU  - Lu Y
AD  - Beijing Municipal Center for Food Safety Monitoring and Risk Assessment, Beijing 
      100041, People's Republic of China. Electronic address: luyong0560@126.com.
LA  - eng
PT  - Journal Article
PT  - Research Support, Non-U.S. Gov't
DEP - 20160322
PL  - England
TA  - Food Chem
JT  - Food chemistry
JID - 7702639
RN  - 0 (Environmental Pollutants)
RN  - 0 (Plant Oils)
RN  - 0 (Polycyclic Aromatic Hydrocarbons)
RN  - EC 3.1.1.- (Carboxylic Ester Hydrolases)
RN  - EC 3.1.1.- (phthalate ester hydrolase)
SB  - IM
MH  - Carboxylic Ester Hydrolases/*chemistry
MH  - Environmental Pollutants/*analysis
MH  - Gas Chromatography-Mass Spectrometry/*methods
MH  - Plant Oils/*chemistry
MH  - Polycyclic Aromatic Hydrocarbons/analysis/*chemistry
MH  - Vegetables/*chemistry
OTO - NOTNLM
OT  - Alkylphenols
OT  - Benzo[a]anthracene (PubChem CID: 5954)
OT  - Benzo[a]pyrene (PubChem CID: 2336)
OT  - Benzo[b]fluoranthene (PubChem CID: 9153)
OT  - Bis(2-ethylhexyl) phthalate (PubChem CID: 8343)
OT  - Chrysene (PubChem CID: 9171)
OT  - Dibutyl phthalate (PubChem CID: 3026)
OT  - Diethyl phthalate (PubChem CID: 6781)
OT  - Diisobutyl phthalate (PubChem CID: 6782)
OT  - Diisononyl phthalate (PubChem CID: 590836)
OT  - Dimethyl phthalate (PubChem CID: 8554)
OT  - GC-MS/MS
OT  - Nonylphenol (PubChem CID: 1752)
OT  - Oil analysis
OT  - Phenanthrene (PubChem CID: 995)
OT  - Phthalate esters
OT  - Polycyclic aromatic hydrocarbons
EDAT- 2016/04/16 06:00
MHDA- 2016/12/15 06:00
CRDT- 2016/04/16 06:00
PHST- 2015/11/20 00:00 [received]
PHST- 2016/03/12 00:00 [revised]
PHST- 2016/03/20 00:00 [accepted]
PHST- 2016/04/16 06:00 [entrez]
PHST- 2016/04/16 06:00 [pubmed]
PHST- 2016/12/15 06:00 [medline]
AID - S0308-8146(16)30444-7 [pii]
AID - 10.1016/j.foodchem.2016.03.071 [doi]
PST - ppublish
SO  - Food Chem. 2016 Sep 15;207:43-50. doi: 10.1016/j.foodchem.2016.03.071. Epub 2016 
      Mar 22.