PMID- 27732757
OWN - NLM
STAT- PubMed-not-MEDLINE
LR  - 20191120
IS  - 1750-3841 (Electronic)
IS  - 0022-1147 (Linking)
VI  - 81
IP  - 11
DP  - 2016 Nov
TI  - Quantitative Analysis of 10 Mycotoxins in Wheat Flour by Ultrahigh Performance 
      Liquid Chromatography-Tandem Mass Spectrometry with a Modified QuEChERS Strategy.
PG  - T2886-T2890
LID - 10.1111/1750-3841.13524 [doi]
AB  - A simple and sensitive analytical method for quantitative analysis of 10 
      mycotoxins was developed and validated by a combination of modified QuEChERS 
      (quick, easy, cheap, effective, rugged, and safe) procedure with ultrahigh 
      performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS). Sample 
      preparation involved QuEChERS with dispersive solid phase extraction for 
      clean-up, and analysis was performed by reversed-phase UHPLC-MS/MS using 
      electrospray negative ionization and multiple reaction monitoring. Under 
      optimized conditions, the calibration curves displayed good linear relationships 
      with all coefficients of determinations (r(2) ) higher than 0.998. The limits of 
      quantification for all target mycotoxins were lower than 7 mug/kg. Trueness and 
      precision for the analytes were 70% to 116% average recoveries and 2% to 13% 
      relative standard deviations (RSDs). The validated method was used to analyze 46 
      wheat flour samples for the targeted mycotoxins. The method can be used as a 
      rapid and robust tool for screening mycotoxin in cereal products.
CI  - (c) 2016 Institute of Food Technologists(R).
FAU - Zhou, Qingxin
AU  - Zhou Q
AD  - Inst. of Agro-Food Science & Technology, Shandong Academy of Agricultural 
      Sciences/Shandong Provincial Key Laboratory of Deep Processing Technology of 
      Agricultural Product, 250100, Jinan, People's Republic of China.
FAU - Li, Fenghua
AU  - Li F
AD  - Inst. of Agro-Food Science & Technology, Shandong Academy of Agricultural 
      Sciences/Shandong Provincial Key Laboratory of Deep Processing Technology of 
      Agricultural Product, 250100, Jinan, People's Republic of China.
AD  - Dept. of Chemistry and Physics, Shandong Center for Food Safety Risk Assessment, 
      Shandong Center for Disease Control and Prevention, 250014, Jinan, People's 
      Republic of China.
FAU - Chen, Leilei
AU  - Chen L
AD  - Inst. of Agro-Food Science & Technology, Shandong Academy of Agricultural 
      Sciences/Shandong Provincial Key Laboratory of Deep Processing Technology of 
      Agricultural Product, 250100, Jinan, People's Republic of China.
FAU - Jiang, Dafeng
AU  - Jiang D
AD  - Inst. of Agro-Food Science & Technology, Shandong Academy of Agricultural 
      Sciences/Shandong Provincial Key Laboratory of Deep Processing Technology of 
      Agricultural Product, 250100, Jinan, People's Republic of China.
AD  - Dept. of Chemistry and Physics, Shandong Center for Food Safety Risk Assessment, 
      Shandong Center for Disease Control and Prevention, 250014, Jinan, People's 
      Republic of China.
LA  - eng
GR  - 2014QNM20/Shandong Academy of Agricultural Sciences/
GR  - 2014WS0382, 2015WS0283/Health and Family Planning Commission of Shandong 
      Province/
GR  - 2015-316/Science and Technology Development Program of Traditional Chinese 
      Medicine of Shandong Province/
PT  - Journal Article
DEP - 20161012
PL  - United States
TA  - J Food Sci
JT  - Journal of food science
JID - 0014052
OTO - NOTNLM
OT  - QuEChERS
OT  - UHPLC-MS/MS
OT  - cereal products
OT  - mycotoxins
OT  - quantitative analysis
EDAT- 2016/10/13 06:00
MHDA- 2016/10/13 06:01
CRDT- 2016/10/13 06:00
PHST- 2016/05/26 00:00 [received]
PHST- 2016/08/17 00:00 [revised]
PHST- 2016/09/11 00:00 [accepted]
PHST- 2016/10/13 06:00 [pubmed]
PHST- 2016/10/13 06:01 [medline]
PHST- 2016/10/13 06:00 [entrez]
AID - 10.1111/1750-3841.13524 [doi]
PST - ppublish
SO  - J Food Sci. 2016 Nov;81(11):T2886-T2890. doi: 10.1111/1750-3841.13524. Epub 2016 
      Oct 12.