PMID- 27769420
OWN - NLM
STAT- PubMed-not-MEDLINE
DCOM- 20180123
LR  - 20180123
IS  - 1873-3573 (Electronic)
IS  - 0039-9140 (Linking)
VI  - 161
DP  - 2016 Dec 1
TI  - Preparation of a new polymeric ionic liquid-based sorbent for stir cake sorptive 
      extraction of trace antimony in environmental water samples.
PG  - 377-383
LID - S0039-9140(16)30639-7 [pii]
LID - 10.1016/j.talanta.2016.08.063 [doi]
AB  - In this work, a new polymeric ionic liquid (PIL)-based sorbent was prepared by 
      in-situ polymerization of 3-(1-ethyl imidazolium-3-yl) propyl-methacrylamido 
      bromide and ethylene dimethacrylate and was used as medium for stir cake sorptive 
      extraction (SCSE) of trace antimony in environmental water samples. The sorbent 
      EPBED was characterized with infrared spectroscopy, elemental analysis, scanning 
      electron microscopy and mercury intrusion porosimetry. A method for determination 
      of trace antimony in water samples was developed based on the combination of 
      SCSE/EPBED and hydride generation atomic fluorescence spectrometry (HG-AFS). 
      Under the optimal extraction conditions, the linear dynamic range of developed 
      method was found to be 0.20-100.0mug/L with good coefficients of correlation 
      (R(2)=0.9904) and LOD value as low as 0.084mug/L. The method showed good 
      reproducibility of results in terms of intra- and inter-day precisions with 
      corresponding relative standard deviations (RSDs) of less than 9%. Recoveries 
      obtained for the determination of antimony in spiked samples ranged from 80.4% to 
      107% with RSDs below 10% in all cases.
CI  - Copyright (c) 2016 Elsevier B.V. All rights reserved.
FAU - Zhang, Yong
AU  - Zhang Y
AD  - State Key Laboratory of Marine Environmental Science, Key Laboratory of the 
      Ministry of Education for Coastal and Wetland Ecosystem, College of the 
      Environment and Ecology, Xiamen University, Xiamen, 361005 China.
FAU - Mei, Meng
AU  - Mei M
AD  - State Key Laboratory of Marine Environmental Science, Key Laboratory of the 
      Ministry of Education for Coastal and Wetland Ecosystem, College of the 
      Environment and Ecology, Xiamen University, Xiamen, 361005 China.
FAU - Ouyang, Tong
AU  - Ouyang T
AD  - State Key Laboratory of Marine Environmental Science, Key Laboratory of the 
      Ministry of Education for Coastal and Wetland Ecosystem, College of the 
      Environment and Ecology, Xiamen University, Xiamen, 361005 China.
FAU - Huang, Xiaojia
AU  - Huang X
AD  - State Key Laboratory of Marine Environmental Science, Key Laboratory of the 
      Ministry of Education for Coastal and Wetland Ecosystem, College of the 
      Environment and Ecology, Xiamen University, Xiamen, 361005 China; Shenzhen 
      Research Institute of Xiamen University, Shenzhen, China. Electronic address: 
      hxj@xmu.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20160823
PL  - Netherlands
TA  - Talanta
JT  - Talanta
JID - 2984816R
OTO - NOTNLM
OT  - Antimony
OT  - Atomic fluorescence spectrometry
OT  - Polymeric ionic liquid
OT  - Stir cake sorptive extraction
OT  - Water
EDAT- 2016/10/23 06:00
MHDA- 2016/10/23 06:01
CRDT- 2016/10/23 06:00
PHST- 2016/07/16 00:00 [received]
PHST- 2016/08/16 00:00 [revised]
PHST- 2016/08/21 00:00 [accepted]
PHST- 2016/10/23 06:00 [pubmed]
PHST- 2016/10/23 06:01 [medline]
PHST- 2016/10/23 06:00 [entrez]
AID - S0039-9140(16)30639-7 [pii]
AID - 10.1016/j.talanta.2016.08.063 [doi]
PST - ppublish
SO  - Talanta. 2016 Dec 1;161:377-383. doi: 10.1016/j.talanta.2016.08.063. Epub 2016 
      Aug 23.