PMID- 27916136
OWN - NLM
STAT- MEDLINE
DCOM- 20180613
LR  - 20181202
IS  - 1873-4324 (Electronic)
IS  - 0003-2670 (Linking)
VI  - 950
DP  - 2017 Jan 15
TI  - A high-throughput screening method of bisphenols, bisphenols digycidyl ethers and 
      their derivatives in dairy products by ultra-high performance liquid 
      chromatography-tandem mass spectrometry.
PG  - 98-107
LID - S0003-2670(16)31291-0 [pii]
LID - 10.1016/j.aca.2016.11.006 [doi]
AB  - A simple and universal analytical method based on ultra-high performance liquid 
      chromatography-tandem mass spectrometry (UHPLC-MS/MS) for high throughput 
      screening of 21 bisphenols, bisphenols digycidyl ethers and their derivatives in 
      dairy products was developed. Response Surface Methodology (RSM) was used to 
      optimize sample preparation conditions based on a quick, easy, cheap, effective, 
      rugged and safe (QuEChERS) method. The analytes were extracted by using 15 mL 
      acetonitrile with 1% acetic acid, and the extracts were further purified by using 
      190 mg of C18 and 390 mg of PSA. The extracts were analyzed by UHPLC-MS/MS with 
      electrospray ionization (ESI) source. Linearity was assessed by using 
      matrix-matched standard calibration and good correlation coefficients 
      (r(2) > 0.99) were obtained. The limits of quantitation (LOQs) for the analytes 
      ranged from 0.02 to 5 mug kg(-1). The extraction recoveries were in a range of 
      88.2%-108.2%. Good method reproducibility in terms of intra- and inter-day 
      precision was observed, yielding relative standard deviations (RSDs) less than 
      8.9% and 9.9%, respectively. The validation method results revealed that the 
      proposed method was sensitive and reliable. Finally, this method was successfully 
      applied to dairy product analysis.
CI  - Copyright A(c) 2016 Elsevier B.V. All rights reserved.
FAU - Cheng, Yan
AU  - Cheng Y
AD  - Institute of Food Safety, Chinese Academy of Inspection & Quarantine, Beijing 
      100176, China; School of Pharmacy, East China University of Science and 
      Technology, Shanghai 200237, China.
FAU - Nie, Xue-Mei
AU  - Nie XM
AD  - Institute of Food Safety, Chinese Academy of Inspection & Quarantine, Beijing 
      100176, China.
FAU - Wu, Han-Qiu
AU  - Wu HQ
AD  - Institute of Food Safety, Chinese Academy of Inspection & Quarantine, Beijing 
      100176, China.
FAU - Hong, Yun-He
AU  - Hong YH
AD  - Institute of Food Safety, Chinese Academy of Inspection & Quarantine, Beijing 
      100176, China.
FAU - Yang, Bing-Cheng
AU  - Yang BC
AD  - School of Pharmacy, East China University of Science and Technology, Shanghai 
      200237, China.
FAU - Liu, Tong
AU  - Liu T
AD  - Institute of Food Safety, Chinese Academy of Inspection & Quarantine, Beijing 
      100176, China.
FAU - Zhao, Dan
AU  - Zhao D
AD  - Institute of Food Safety, Chinese Academy of Inspection & Quarantine, Beijing 
      100176, China.
FAU - Wang, Jian-Feng
AU  - Wang JF
AD  - Institute of Food Safety, Chinese Academy of Inspection & Quarantine, Beijing 
      100176, China.
FAU - Yao, Gui-Hong
AU  - Yao GH
AD  - Institute of Food Safety, Chinese Academy of Inspection & Quarantine, Beijing 
      100176, China.
FAU - Zhang, Feng
AU  - Zhang F
AD  - Institute of Food Safety, Chinese Academy of Inspection & Quarantine, Beijing 
      100176, China. Electronic address: fengzhang@126.com.
LA  - eng
PT  - Journal Article
DEP - 20161111
PL  - Netherlands
TA  - Anal Chim Acta
JT  - Analytica chimica acta
JID - 0370534
RN  - 0 (Ethers)
RN  - 0 (Phenols)
SB  - IM
MH  - Animals
MH  - Cattle
MH  - Chromatography, High Pressure Liquid
MH  - Dairy Products/*analysis
MH  - Ethers/*analysis
MH  - *High-Throughput Screening Assays
MH  - Phenols/*analysis
MH  - Reproducibility of Results
MH  - Tandem Mass Spectrometry
OTO - NOTNLM
OT  - Bisphenols
OT  - Bisphenols digycidyl ethers and their derivatives
OT  - High throughput
OT  - QuEChERS
OT  - Ultra-high performance liquid chromatography-tandem mass spectrometry
EDAT- 2016/12/06 06:00
MHDA- 2018/06/14 06:00
CRDT- 2016/12/06 06:00
PHST- 2016/08/24 00:00 [received]
PHST- 2016/10/27 00:00 [revised]
PHST- 2016/11/01 00:00 [accepted]
PHST- 2016/12/06 06:00 [entrez]
PHST- 2016/12/06 06:00 [pubmed]
PHST- 2018/06/14 06:00 [medline]
AID - S0003-2670(16)31291-0 [pii]
AID - 10.1016/j.aca.2016.11.006 [doi]
PST - ppublish
SO  - Anal Chim Acta. 2017 Jan 15;950:98-107. doi: 10.1016/j.aca.2016.11.006. Epub 2016 
      Nov 11.