PMID- 27916955
OWN - NLM
STAT- MEDLINE
DCOM- 20170407
LR  - 20200225
IS  - 1420-3049 (Electronic)
IS  - 1420-3049 (Linking)
VI  - 21
IP  - 12
DP  - 2016 Dec 1
TI  - Multi-Residue Analysis of Pesticide Residues in Crude Pollens by UPLC-MS/MS.
LID - 1652
AB  - A multi-residue method for the determination of 54 pesticide residues in pollens 
      has been developed and validated. The proposed method was applied to the analysis 
      of 48 crude pollen samples collected from eight provinces of China. The recovery 
      of analytes ranged from 60% to 136% with relative standard deviations (RSDs) 
      below 30%. Of the 54 targeted compounds, 19 pesticides were detected. The major 
      detection rates of each compound were 77.1% for carbendazim, 58.3% for 
      fenpropathrin, 56.3% for chlorpyrifos, 50.0% for fluvalinate, 31.3% for 
      chlorbenzuron, and 29.2% for triadimefon in crude pollen samples. The maximum 
      values of each pesticide were 4516 ng/g for carbendazim, 162.8 ng/g for 
      fenpropathrin, 176.6 ng/g for chlorpyrifos, 316.2 ng/g for fluvalinate, 437.2 
      ng/g for chlorbenzuron, 79.00 ng/g for triadimefon, and so on. This study 
      provides basis for the research on the risks to honeybee health.
FAU - Tong, Zhou
AU  - Tong Z
AD  - School of Plant Protection, Anhui Agricultural University, Hefei 230036, China. 
      tongzhou0520@163.com.
FAU - Wu, Yan-Can
AU  - Wu YC
AD  - School of Plant Protection, Anhui Agricultural University, Hefei 230036, China. 
      wuyancan1989@163.com.
AD  - Hefei Testing and Inspection Center for Agricultural Products Quality, Hefei 
      230601, China. wuyancan1989@163.com.
FAU - Liu, Qiong-Qiong
AU  - Liu QQ
AD  - School of Plant Protection, Anhui Agricultural University, Hefei 230036, China. 
      ahbb1104@163.com.
FAU - Shi, Yan-Hong
AU  - Shi YH
AD  - School of Plant Protection, Anhui Agricultural University, Hefei 230036, China. 
      shiyh@ahau.edu.cn.
FAU - Zhou, Li-Jun
AU  - Zhou LJ
AD  - School of Plant Protection, Anhui Agricultural University, Hefei 230036, China. 
      ljzhou0720@163.com.
FAU - Liu, Zhen-Yu
AU  - Liu ZY
AD  - School of Plant Protection, Anhui Agricultural University, Hefei 230036, China. 
      zliu@ahau.edu.cn.
FAU - Yu, Lin-Sheng
AU  - Yu LS
AD  - School of Plant Protection, Anhui Agricultural University, Hefei 230036, China. 
      yulinsheng@ahau.edu.cn.
FAU - Cao, Hai-Qun
AU  - Cao HQ
AD  - School of Plant Protection, Anhui Agricultural University, Hefei 230036, China. 
      haiquncao@163.com.
LA  - eng
PT  - Journal Article
DEP - 20161201
PL  - Switzerland
TA  - Molecules
JT  - Molecules (Basel, Switzerland)
JID - 100964009
RN  - 0 (Pesticides)
SB  - IM
MH  - China
MH  - Pesticides/*analysis/chemistry
MH  - Pollen/*chemistry
PMC - PMC6273886
OTO - NOTNLM
OT  - UPLC-MS/MS
OT  - multi-residue
OT  - pesticide
OT  - pollen
COIS- The authors declare no conflict of interest.
EDAT- 2016/12/06 06:00
MHDA- 2017/04/08 06:00
PMCR- 2016/12/01
CRDT- 2016/12/06 06:00
PHST- 2016/11/06 00:00 [received]
PHST- 2016/11/24 00:00 [revised]
PHST- 2016/11/24 00:00 [accepted]
PHST- 2016/12/06 06:00 [entrez]
PHST- 2016/12/06 06:00 [pubmed]
PHST- 2017/04/08 06:00 [medline]
PHST- 2016/12/01 00:00 [pmc-release]
AID - molecules21121652 [pii]
AID - molecules-21-01652 [pii]
AID - 10.3390/molecules21121652 [doi]
PST - epublish
SO  - Molecules. 2016 Dec 1;21(12):1652. doi: 10.3390/molecules21121652.