PMID- 28025454
OWN - NLM
STAT- MEDLINE
DCOM- 20170308
LR  - 20171016
IS  - 1882-1006 (Electronic)
IS  - 0015-6426 (Linking)
VI  - 57
IP  - 6
DP  - 2016
TI  - [Determination of Diphenylamine in Agricultural Products by HPLC-FL].
PG  - 201-206
LID - 10.3358/shokueishi.57.201 [doi]
AB  - A method for the determination of diphenylamine in agricultural products was 
      developed. Diphenylamine was extracted with acetonitrile from a sample under an 
      acidic condition, passed through a C18 cartridge column, re-extracted with 
      n-hexane, cleaned up on a PSA cartridge column, determined by HPLC with 
      fluorescence detector and confirmed by liquid chromatography with tandem mass 
      spectrometry. Average recoveries (n=5) from brown rice, corn, soybeans, potato, 
      cabbage, eggplant, spinach, orange, apple and green tea were in the range from 
      76.7 to 94.9%, and the relative standard deviations were from 0.6 to 5.8% at 
      concentrations equal to the maximum residue limits (MRLs). The quantification 
      limits were 0.01 mg/kg, which is the uniform limit in the positive list system 
      for agricultural chemical residues in food in Japan.
FAU - Aoyagi, Mitsutoshi
AU  - Aoyagi M
AD  - Hokkaido Institute of Public Health.
FAU - Chiba, Masahiro
AU  - Chiba M
FAU - Kakimoto, Youichiro
AU  - Kakimoto Y
FAU - Nemoto, Satoru
AU  - Nemoto S
LA  - jpn
PT  - Journal Article
PL  - Japan
TA  - Shokuhin Eiseigaku Zasshi
JT  - Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan
JID - 0142214
RN  - 0 (Acetonitriles)
RN  - 0 (Hexanes)
RN  - 0 (Pesticide Residues)
RN  - 2DDG612ED8 (n-hexane)
RN  - 9N3CBB0BIQ (Diphenylamine)
RN  - Z072SB282N (acetonitrile)
SB  - IM
MH  - Acetonitriles
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Chromatography, Liquid
MH  - Crops, Agricultural/*chemistry
MH  - Diphenylamine/*analysis/isolation & purification
MH  - Fluorescence
MH  - Food Analysis/*methods
MH  - Hexanes
MH  - Pesticide Residues/*analysis/isolation & purification
MH  - Tandem Mass Spectrometry
EDAT- 2016/12/28 06:00
MHDA- 2017/03/09 06:00
CRDT- 2016/12/28 06:00
PHST- 2016/12/28 06:00 [entrez]
PHST- 2016/12/28 06:00 [pubmed]
PHST- 2017/03/09 06:00 [medline]
AID - 10.3358/shokueishi.57.201 [doi]
PST - ppublish
SO  - Shokuhin Eiseigaku Zasshi. 2016;57(6):201-206. doi: 10.3358/shokueishi.57.201.