PMID- 28292733
OWN - NLM
STAT- MEDLINE
DCOM- 20170601
LR  - 20170601
IS  - 1873-376X (Electronic)
IS  - 1570-0232 (Linking)
VI  - 1051
DP  - 2017 Apr 15
TI  - Rapid determination of 54 pharmaceutical and personal care products in fish 
      samples using microwave-assisted extraction-Hollow fiber-Liquid/solid phase 
      microextraction.
PG  - 41-53
LID - S1570-0232(16)31035-2 [pii]
LID - 10.1016/j.jchromb.2017.01.026 [doi]
AB  - In this paper, a simple, rapid, solvent-less and environmental friendliness 
      microextraction method, microwave-assisted extraction-hollow fiber-liquid/solid 
      phase microextraction (MAE-HF-L/SME), was developed for simultaneous extraction 
      and enrichment of 54 trace hydrophilic/lipophilic pharmaceutical and personal 
      care products (PPCPs) from fish samples. A solid-phase extraction material, 
      solid-phase microextraction (SPME) fiber, was synthesized. The SPME fiber had a 
      homogeneous, loose structure and good mechanical properties, and they exhibited a 
      good adsorption capacity for most PPCPs selected. The material formed the basis 
      for the method of MAE-HF-L/SME. A method of liquid chromatography-high resolution 
      mass spectroscopy (LC-HRMS) for analysis of 54 PPCPs. Under optimal synthesis and 
      extraction conditions, the limits of detection (LODs, n=3) and the limits of 
      quantitation (LOQs, n=10) for the 54 PPCPs were between 0.01-0.50mug.kg(-1) and 
      0.052.00mug.kg(-1), respectively. Percent recoveries and the relative standard 
      deviations (RSDs) in spiked fish samples (n=6) were between 56.3%-119.9% and 
      0.3%-17.1%, respectively. The microextraction process of 54 PPCPs in MAE-HF-L/SME 
      took approximately 12min. The method has a low matrix interference and high 
      enrichment factor and may be applicable for determination of 54 different PPCPs 
      in fish samples.
CI  - Copyright (c) 2017 Elsevier B.V. All rights reserved.
FAU - Zhang, Yi
AU  - Zhang Y
AD  - Food Inspection and Quarantine Technology Center, Shenzhen Entry-Exit Inspection 
      and Quarantine Bureau of China, Shenzhen, Guangdong, PR China. Electronic 
      address: zhayi80@gmail.com.
FAU - Guo, Wen
AU  - Guo W
AD  - Food Inspection and Quarantine Technology Center, Shenzhen Entry-Exit Inspection 
      and Quarantine Bureau of China, Shenzhen, Guangdong, PR China; School of 
      Chemistry and Environment Engineering Shenzhen University, Shenzhen, Guangdong, 
      PR China.
FAU - Yue, Zhenfeng
AU  - Yue Z
AD  - Food Inspection and Quarantine Technology Center, Shenzhen Entry-Exit Inspection 
      and Quarantine Bureau of China, Shenzhen, Guangdong, PR China.
FAU - Lin, Li
AU  - Lin L
AD  - Food Inspection and Quarantine Technology Center, Shenzhen Entry-Exit Inspection 
      and Quarantine Bureau of China, Shenzhen, Guangdong, PR China.
FAU - Zhao, Fengjuan
AU  - Zhao F
AD  - Food Inspection and Quarantine Technology Center, Shenzhen Entry-Exit Inspection 
      and Quarantine Bureau of China, Shenzhen, Guangdong, PR China.
FAU - Chen, Peijin
AU  - Chen P
AD  - Food Inspection and Quarantine Technology Center, Shenzhen Entry-Exit Inspection 
      and Quarantine Bureau of China, Shenzhen, Guangdong, PR China.
FAU - Wu, Weidong
AU  - Wu W
AD  - Food Inspection and Quarantine Technology Center, Shenzhen Entry-Exit Inspection 
      and Quarantine Bureau of China, Shenzhen, Guangdong, PR China.
FAU - Zhu, Hong
AU  - Zhu H
AD  - School of Chemistry and Environment Engineering Shenzhen University, Shenzhen, 
      Guangdong, PR China.
FAU - Yang, Bo
AU  - Yang B
AD  - School of Chemistry and Environment Engineering Shenzhen University, Shenzhen, 
      Guangdong, PR China.
FAU - Kuang, Yanyun
AU  - Kuang Y
AD  - Food Inspection and Quarantine Technology Center, Shenzhen Entry-Exit Inspection 
      and Quarantine Bureau of China, Shenzhen, Guangdong, PR China.
FAU - Wang, Jiong
AU  - Wang J
AD  - Food Inspection and Quarantine Technology Center, Shenzhen Entry-Exit Inspection 
      and Quarantine Bureau of China, Shenzhen, Guangdong, PR China.
LA  - eng
PT  - Journal Article
DEP - 20170121
PL  - Netherlands
TA  - J Chromatogr B Analyt Technol Biomed Life Sci
JT  - Journal of chromatography. B, Analytical technologies in the biomedical and life 
      sciences
JID - 101139554
RN  - 0 (Cosmetics)
RN  - 0 (Pharmaceutical Preparations)
RN  - 0 (Water Pollutants, Chemical)
SB  - IM
MH  - Animals
MH  - Chromatography, Liquid/methods
MH  - Cosmetics/*analysis
MH  - Equipment Design
MH  - Fishes/*metabolism
MH  - Limit of Detection
MH  - Liquid Phase Microextraction/instrumentation/methods
MH  - Mass Spectrometry/methods
MH  - Microwaves
MH  - Pharmaceutical Preparations/*analysis
MH  - Solid Phase Microextraction/instrumentation/*methods
MH  - Water Pollutants, Chemical/*analysis
OTO - NOTNLM
OT  - Hollow fiber-liquid/solid phase microextraction
OT  - Liquid chromatography-high resolution mass spectroscopy (LC-HRMS)
OT  - Microwave-assisted extraction (MAE)
OT  - Pharmaceutical and personal care products (PPCPs)
OT  - Solid-phase microextraction fiber
EDAT- 2017/03/16 06:00
MHDA- 2017/06/02 06:00
CRDT- 2017/03/16 06:00
PHST- 2016/10/12 00:00 [received]
PHST- 2017/01/11 00:00 [revised]
PHST- 2017/01/19 00:00 [accepted]
PHST- 2017/03/16 06:00 [pubmed]
PHST- 2017/06/02 06:00 [medline]
PHST- 2017/03/16 06:00 [entrez]
AID - S1570-0232(16)31035-2 [pii]
AID - 10.1016/j.jchromb.2017.01.026 [doi]
PST - ppublish
SO  - J Chromatogr B Analyt Technol Biomed Life Sci. 2017 Apr 15;1051:41-53. doi: 
      10.1016/j.jchromb.2017.01.026. Epub 2017 Jan 21.