PMID- 28338342
OWN - NLM
STAT- MEDLINE
DCOM- 20171130
LR  - 20181202
IS  - 1478-6427 (Electronic)
IS  - 1478-6419 (Linking)
VI  - 31
IP  - 15
DP  - 2017 Aug
TI  - Development of matrix solid-phase dispersion coupled with high-performance liquid 
      chromatography for determination of jolkinolide A and jolkinolide B in Euphorbia 
      fischeriana Steud.
PG  - 1805-1811
LID - 10.1080/14786419.2017.1297993 [doi]
AB  - A novel and simple method was established for the extraction and determination of 
      jolkinolide A and B in Euphorbia fischeriana Steud. using matrix solid-phase 
      dispersion (MSPD) extraction and high-performance liquid chromatography (HPLC). 
      The optimised conditions for the MSPD extraction were determined to be that 
      silica gel was served as dispersant, the mass ratio of sample to silica gel was 
      selected to be 1:4, and 5 mL of acetonitrile was used as elution solvent. The 
      method exhibited a good performance in terms of linearity (r(2) >/= 0.9997) and the 
      limits of detection in the range of 0.052-0.065 mug mL(-1). The recoveries were in 
      the range of 90.2-98.9% with relative standard deviations (RSDs) ranging from 1.3 
      to 3.5%. The extraction efficiencies obtained by the MSPD were higher than other 
      extraction method with less cost of sample and solvent. At last, the optimised 
      method was applied for analysing real samples.
FAU - Cai, Defu
AU  - Cai D
AD  - a Institute of Medicine and Drug Research , Qiqihar Medical University , Qiqihar 
      , China.
FAU - Zhai, Weiyu
AU  - Zhai W
AD  - b The First Affiliated Hospital , Qiqihar Medical University , Qiqihar , China.
FAU - Zhang, Qi
AU  - Zhang Q
AD  - a Institute of Medicine and Drug Research , Qiqihar Medical University , Qiqihar 
      , China.
FAU - Liu, Jianhua
AU  - Liu J
AD  - a Institute of Medicine and Drug Research , Qiqihar Medical University , Qiqihar 
      , China.
FAU - Sun, Yu
AU  - Sun Y
AD  - a Institute of Medicine and Drug Research , Qiqihar Medical University , Qiqihar 
      , China.
FAU - Liu, Lei
AU  - Liu L
AD  - a Institute of Medicine and Drug Research , Qiqihar Medical University , Qiqihar 
      , China.
FAU - Liu, Jicheng
AU  - Liu J
AD  - a Institute of Medicine and Drug Research , Qiqihar Medical University , Qiqihar 
      , China.
LA  - eng
PT  - Journal Article
DEP - 20170324
PL  - England
TA  - Nat Prod Res
JT  - Natural product research
JID - 101167924
RN  - 0 (Diterpenes)
RN  - 0 (Solvents)
RN  - 37905-07-0 (jolkinolide A)
RN  - 37905-08-1 (jolkinolide B)
SB  - IM
MH  - Chromatography, High Pressure Liquid/*methods
MH  - Diterpenes/*analysis
MH  - Euphorbia/*chemistry
MH  - Limit of Detection
MH  - Solid Phase Extraction/*methods
MH  - Solvents
OTO - NOTNLM
OT  - Euphorbia fischeriana Steud
OT  - Matrix solid-phase dispersion
OT  - jolkinolide A
OT  - jolkinolide B
OT  - liquid chromatography
EDAT- 2017/03/25 06:00
MHDA- 2017/12/01 06:00
CRDT- 2017/03/25 06:00
PHST- 2017/03/25 06:00 [pubmed]
PHST- 2017/12/01 06:00 [medline]
PHST- 2017/03/25 06:00 [entrez]
AID - 10.1080/14786419.2017.1297993 [doi]
PST - ppublish
SO  - Nat Prod Res. 2017 Aug;31(15):1805-1811. doi: 10.1080/14786419.2017.1297993. Epub 
      2017 Mar 24.