PMID- 28372183
OWN - NLM
STAT- MEDLINE
DCOM- 20170505
LR  - 20181202
IS  - 1873-7072 (Electronic)
IS  - 0308-8146 (Linking)
VI  - 229
DP  - 2017 Aug 15
TI  - Simultaneous determination of pesticide residues and antioxidants in blended oil 
      using a liquid-liquid extraction combined with dispersive solid phase extraction 
      method.
PG  - 347-353
LID - S0308-8146(17)30295-9 [pii]
LID - 10.1016/j.foodchem.2017.02.094 [doi]
AB  - This article developed a method to detect two antioxidants (butylated hydroxyl 
      anisole (BHA), butylated hydroxyl toluene (BHT)) and twelve pesticides 
      (dichlorvos, pirimicarb, prothiofos, fenitrothion, ethoprophos, malathion, 
      beta-Cypermethrin, profenofos, diazinon, propoxur, procymidon, captan) in blended 
      oil samples after their extraction simultaneously. The establishment of the 
      method was based on two-step process of screening and optimization experiment 
      design. With a Plackett-Burman (PB) design, significant parameters were found by 
      screening experiment and single factor experiment accompanied by a central 
      composite design (CCD) experiment were used to make important parameters optimal. 
      The coefficients of determination (r(2)) was between 0.9931 and 0.9996 while the 
      limits of quantification (LOQs) and limits of detection (LODs) were found in 
      scope of 0.002-0.04mg.kg(-1) and 0.0006-0.0012mg.kg(-1). Recovery values of 
      analytes were above 74%, at the same time the relative standard deviations (RSDs) 
      under 10% at the concentrations ranging from 0.05mg.kg(-1) to 0.20mg.kg(-1). To 
      sum up, this method with shorter time and fewer consumption of reagents could be 
      employed in various occasions to detect antioxidants and pesticides.
CI  - Copyright (c) 2017 Elsevier Ltd. All rights reserved.
FAU - Fang, Yong
AU  - Fang Y
AD  - College of Food Science and Engineering/Collaborative Innovation Center for 
      Modern Grain Circulation and Safety/Key Laboratory of Grains and Oils Quality 
      Control and Processing, Nanjing University of Finance and Economics, Nanjing 
      210023, China.
FAU - Tian, Wen
AU  - Tian W
AD  - College of Food Science and Engineering/Collaborative Innovation Center for 
      Modern Grain Circulation and Safety/Key Laboratory of Grains and Oils Quality 
      Control and Processing, Nanjing University of Finance and Economics, Nanjing 
      210023, China.
FAU - Pei, Fei
AU  - Pei F
AD  - College of Food Science and Engineering/Collaborative Innovation Center for 
      Modern Grain Circulation and Safety/Key Laboratory of Grains and Oils Quality 
      Control and Processing, Nanjing University of Finance and Economics, Nanjing 
      210023, China.
FAU - Li, Peng
AU  - Li P
AD  - College of Food Science and Engineering/Collaborative Innovation Center for 
      Modern Grain Circulation and Safety/Key Laboratory of Grains and Oils Quality 
      Control and Processing, Nanjing University of Finance and Economics, Nanjing 
      210023, China.
FAU - Shao, XiaoLong
AU  - Shao X
AD  - College of Food Science and Engineering/Collaborative Innovation Center for 
      Modern Grain Circulation and Safety/Key Laboratory of Grains and Oils Quality 
      Control and Processing, Nanjing University of Finance and Economics, Nanjing 
      210023, China.
FAU - Fan, Yan
AU  - Fan Y
AD  - College of Food Science and Engineering/Collaborative Innovation Center for 
      Modern Grain Circulation and Safety/Key Laboratory of Grains and Oils Quality 
      Control and Processing, Nanjing University of Finance and Economics, Nanjing 
      210023, China.
FAU - Hu, Qiuhui
AU  - Hu Q
AD  - College of Food Science and Engineering/Collaborative Innovation Center for 
      Modern Grain Circulation and Safety/Key Laboratory of Grains and Oils Quality 
      Control and Processing, Nanjing University of Finance and Economics, Nanjing 
      210023, China. Electronic address: qiuhuihu@njue.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20170221
PL  - England
TA  - Food Chem
JT  - Food chemistry
JID - 7702639
RN  - 0 (Antioxidants)
RN  - 0 (Pesticide Residues)
SB  - IM
MH  - Antioxidants/*analysis
MH  - Liquid-Liquid Extraction/*methods
MH  - Pesticide Residues/*analysis
MH  - Solid Phase Extraction/*methods
OTO - NOTNLM
OT  - Antioxidants
OT  - Central composite design
OT  - Dispersive solid phase extraction
OT  - Pesticides
OT  - Plackett-Burman experiment
EDAT- 2017/04/05 06:00
MHDA- 2017/05/06 06:00
CRDT- 2017/04/05 06:00
PHST- 2016/06/23 00:00 [received]
PHST- 2017/01/16 00:00 [revised]
PHST- 2017/02/18 00:00 [accepted]
PHST- 2017/04/05 06:00 [entrez]
PHST- 2017/04/05 06:00 [pubmed]
PHST- 2017/05/06 06:00 [medline]
AID - S0308-8146(17)30295-9 [pii]
AID - 10.1016/j.foodchem.2017.02.094 [doi]
PST - ppublish
SO  - Food Chem. 2017 Aug 15;229:347-353. doi: 10.1016/j.foodchem.2017.02.094. Epub 
      2017 Feb 21.