PMID- 28385122
OWN - NLM
STAT- MEDLINE
DCOM- 20171016
LR  - 20191210
IS  - 1944-0057 (Electronic)
IS  - 1944-0057 (Linking)
VI  - 34
IP  - 7
DP  - 2017 Jul
TI  - Development and validation of a solid-phase extraction method coupled with 
      HPLC-UV detection for the determination of biogenic amines in Chinese rice wine.
PG  - 1172-1183
LID - 10.1080/19440049.2017.1317366 [doi]
AB  - A reliable and accurate method for the determination of seven biogenic amines 
      (BAs) was developed and validated with Chinese rice wine samples. The BAs were 
      derivatised with dansyl chloride, cleaned up using solid-phase extraction (SPE) 
      and separated by high-performance liquid chromatography (HPLC) coupled with 
      ultraviolet (UV) detection. The optimised derivatisation reaction, conducted at 
      pH 9.6 and 60 degrees C for 30 min, ensured baseline separation and peak symmetry for 
      each BA. SPE clean-up using Oasis MCX cartridges yielded good recovery rates for 
      all BAs and effectively reduced matrix effects. The developed method shows good 
      linearity with determination coefficients of more than 0.9989 over a 
      concentration range of 0.1-100 mg l(-1). The limits of detection (LODs) for the 
      investigated BAs ranged from 2.07 to 5.56 microg l(-1). The intra- and inter-day 
      relative standard deviations (RSDs) ranged from 0.86% to 3.81% and from 2.13% to 
      3.82%, respectively. Spiking experiments showed that the overall recovery rates 
      ranged from 85% to 113%. Thus, the proposed method was demonstrated as being 
      suitable for simultaneous detection, with accurate and precise quantification, of 
      BAs in Chinese rice wine.
FAU - Zhang, Ying
AU  - Zhang Y
AD  - a Key Laboratory of Food Nutrition and Safety, Ministry of Education , Tianjin 
      University of Science and Technology , Tianjin , China.
FAU - Li, Yan
AU  - Li Y
AD  - a Key Laboratory of Food Nutrition and Safety, Ministry of Education , Tianjin 
      University of Science and Technology , Tianjin , China.
FAU - Zhu, Xiao-Juan
AU  - Zhu XJ
AD  - b Tianjin Industrial Microbiology Key Laboratory, College of Biotechnology , 
      Tianjin University of Science and Technology , Tianjin , China.
FAU - Li, Min
AU  - Li M
AD  - c College of Chemical Engineering and Materials Science , Tianjin University of 
      Science and Technology , Tianjin , China.
FAU - Chen, Hao-Yu
AU  - Chen HY
AD  - b Tianjin Industrial Microbiology Key Laboratory, College of Biotechnology , 
      Tianjin University of Science and Technology , Tianjin , China.
FAU - Lv, Xiao-Ling
AU  - Lv XL
AD  - a Key Laboratory of Food Nutrition and Safety, Ministry of Education , Tianjin 
      University of Science and Technology , Tianjin , China.
FAU - Zhang, Jian
AU  - Zhang J
AD  - b Tianjin Industrial Microbiology Key Laboratory, College of Biotechnology , 
      Tianjin University of Science and Technology , Tianjin , China.
AD  - d Tianjin SF-Bio Industrial Bio-Tec Co., Ltd , Tianjin , China.
LA  - eng
PT  - Journal Article
PT  - Validation Study
DEP - 20170517
PL  - England
TA  - Food Addit Contam Part A Chem Anal Control Expo Risk Assess
JT  - Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & 
      risk assessment
JID - 101485040
RN  - 0 (Biogenic Amines)
SB  - IM
MH  - Biogenic Amines/*analysis
MH  - China
MH  - Chromatography, High Pressure Liquid
MH  - Oryza/*chemistry
MH  - Solid Phase Extraction/*methods
MH  - *Ultraviolet Rays
MH  - Wine/*analysis
OTO - NOTNLM
OT  - Biogenic amines
OT  - Chinese rice wine
OT  - high-performance liquid chromatography
OT  - matrix effects
OT  - solid-phase extraction
EDAT- 2017/04/08 06:00
MHDA- 2017/10/17 06:00
CRDT- 2017/04/08 06:00
PHST- 2017/04/08 06:00 [pubmed]
PHST- 2017/10/17 06:00 [medline]
PHST- 2017/04/08 06:00 [entrez]
AID - 10.1080/19440049.2017.1317366 [doi]
PST - ppublish
SO  - Food Addit Contam Part A Chem Anal Control Expo Risk Assess. 2017 
      Jul;34(7):1172-1183. doi: 10.1080/19440049.2017.1317366. Epub 2017 May 17.