PMID- 28482442 OWN - NLM STAT- MEDLINE DCOM- 20170830 LR - 20181202 IS - 1002-0098 (Print) IS - 1002-0098 (Linking) VI - 52 IP - 5 DP - 2017 May 9 TI - [Effect of a nano hydroxyapatite desensitizing paste application on dentin bond strength of three self-etch adhesive systems]. PG - 278-282 LID - 10.3760/cma.j.issn.1002-0098.2017.05.004 [doi] AB - Objective: To evaluate a nano-hydroxyapatite (nano-HA) desensitizing paste application on the bond strength of three self-etch adhesives. Methods: Three dentin specimens of about 1 mm thick were cut from two teeth. Scanning electron microscope (SEM) was used to evaluate the dentin surfaces without treatment, after citric acid treatment and after nano-HA treatment. Thirty-six intact third molars extracted for surgical reasons were cut to remove the occlusal enamel with isomet, and then were etched with 1% citric acid for 20 s to simulate the sensitive dentin and divided into two groups randomly using a table of random numbers (n=18): the control group (no treatment) and the HA treated group (with nano-HA paste treatment). Each group was divided into three subgroups randomly using a table of random numbers (n=6). Subgroup A, B and C was bonded with G-Bond, Clearfil S(3) Bond and FL-Bond Ⅱ according to the manufacture's instruction separately. At 24 h after bonding procedure, and after water storage for 6 months, microtensile bond strength of the specimens was tested and the failure mode was analyzed. Results: SEM obeservation showed that citric acid could open the dentin tubules to set up the sensitive dentin model, and the nano-HA could occlude the dentin tubules effectively. For subgroup A, bonding strength of specimens treated with nano-HA ([41.14+/-8.91] MPa) was significantly high than that of the control group ([34.27+/-6.16] MPa) at 24 h after bonding procedure (P<0.05). However, after 6 month water ageing, the bonding strength of the control group and the HA treated group showed no significant difference (P>0.05). For subgroup B, specimens with nano-HA application showed lower bonding strength ([30.87+/-6.41] MPa) than that of the control group ([36.73+/-5.82] MPa) at 24 h after bonding procedure (P<0.05), and after 6 month water ageing, the bond strength of nano-HA application ([25.73+/-6.99] MPa) was also lower than that of the control group ([32.33+/-5.08] MPa) (P<0.05). For subgroup C, the bond strength of the control group and the HA treated group have no significant difference either before or after 6 month water ageing (P>0.05). Failure mode analysis showed that more than half of the samples in all groups were adhesive failure. Conclusions: Nano-HA treatment decreased the bond strength of subgroup B, while had no adverse effect on subgroup A and subgroup C. FAU - Pei, D D AU - Pei DD AD - Key Laboratory of Shaanxi Province for Craniofacial Precision Medicine Research, College of Stomatology, Xi'an Jiaotong University, Xi'an 710004, China. FAU - Liu, S Y AU - Liu SY AD - Department of Oral and Maxillofacial Surgery, School of Stomatology, Wuhan University, Wuhan 430079, China. FAU - Yang, H Y AU - Yang HY AD - Department of Prosthodontics, School of Stomatology, Wuhan University, Wuhan 430079, China. FAU - Gan, J AU - Gan J AD - Department of Prosthodontics, College of Stomatology, Xi'an Jiaotong University, Xi'an 710004, China. FAU - Huang, C AU - Huang C AD - Department of Prosthodontics, School of Stomatology, Wuhan University, Wuhan 430079, China. LA - chi PT - Journal Article PL - China TA - Zhonghua Kou Qiang Yi Xue Za Zhi JT - Zhonghua kou qiang yi xue za zhi = Zhonghua kouqiang yixue zazhi = Chinese journal of stomatology JID - 8711066 RN - 0 (Adhesives) RN - 0 (Dentin-Bonding Agents) RN - 0 (G-Bond) RN - 0 (Methacrylates) RN - 0 (Ointments) RN - 91D9GV0Z28 (Durapatite) SB - IM MH - Adhesives MH - *Dental Bonding MH - Dental Enamel/drug effects MH - Dentin/*drug effects MH - Dentin-Bonding Agents MH - *Durapatite MH - Humans MH - Materials Testing MH - Methacrylates MH - Microscopy, Electron, Scanning MH - *Nanoparticles MH - Ointments MH - Random Allocation MH - Tensile Strength/drug effects OTO - NOTNLM OT - Dentin sensitivity OT - Dentin-bonding agents OT - Hydroxyapatites EDAT- 2017/05/10 06:00 MHDA- 2017/08/31 06:00 CRDT- 2017/05/09 06:00 PHST- 2017/05/09 06:00 [entrez] PHST- 2017/05/10 06:00 [pubmed] PHST- 2017/08/31 06:00 [medline] AID - 10.3760/cma.j.issn.1002-0098.2017.05.004 [doi] PST - ppublish SO - Zhonghua Kou Qiang Yi Xue Za Zhi. 2017 May 9;52(5):278-282. doi: 10.3760/cma.j.issn.1002-0098.2017.05.004.