PMID- 28490065
OWN - NLM
STAT- MEDLINE
DCOM- 20170816
LR  - 20181202
IS  - 1873-7072 (Electronic)
IS  - 0308-8146 (Linking)
VI  - 232
DP  - 2017 Oct 1
TI  - Residue analysis of tetracyclines in milk by HPLC coupled with hollow fiber 
      membranes-based dynamic liquid-liquid micro-extraction.
PG  - 198-202
LID - S0308-8146(17)30565-4 [pii]
LID - 10.1016/j.foodchem.2017.04.021 [doi]
AB  - A novel hollow fiber membranes-based dynamic liquid-liquid micro-extraction 
      (HF-DLLME) coupled with HPLC-UV detection has been developed for the residue 
      analysis of tetracyclines in milk samples without deproteinization and 
      degreasing. The influences of experimental parameters were investigated and 
      optimized. The method showed a good performance. The limits of detection (LOD) 
      are in the range of 0.95-3.6mug/L. The recoveries in spiked samples range from 
      92.38 to 107.3%. The relative standard deviations (RSDs) are lower than 8.66%. 
      The advantages of this method are simple operation, high efficiency, absence of 
      sample carryover and low cost.
CI  - Copyright (c) 2017 Elsevier Ltd. All rights reserved.
FAU - Xu, Hui
AU  - Xu H
AD  - Department of Analytical Chemistry, College of Chemistry, Jilin University, 
      Changchun 130021, PR China. Electronic address: xuhui1418@163.com.
FAU - Mi, Hong-Yu
AU  - Mi HY
AD  - Department of Analytical Chemistry, College of Chemistry, Jilin University, 
      Changchun 130021, PR China. Electronic address: mihongyu1992@163.com.
FAU - Guan, Ming-Ming
AU  - Guan MM
AD  - Department of Analytical Chemistry, College of Chemistry, Jilin University, 
      Changchun 130021, PR China. Electronic address: 15530839940@163.com.
FAU - Shan, Hong-Yan
AU  - Shan HY
AD  - Department of Analytical Chemistry, College of Chemistry, Jilin University, 
      Changchun 130021, PR China. Electronic address: shanhy@jlu.edu.cn.
FAU - Fei, Qiang
AU  - Fei Q
AD  - Department of Analytical Chemistry, College of Chemistry, Jilin University, 
      Changchun 130021, PR China. Electronic address: feiqiang@jlu.edu.cn.
FAU - Huan, Yan-Fu
AU  - Huan YF
AD  - Department of Analytical Chemistry, College of Chemistry, Jilin University, 
      Changchun 130021, PR China. Electronic address: yfhuan@jlu.edu.cn.
FAU - Zhang, Zhi-Quan
AU  - Zhang ZQ
AD  - Department of Analytical Chemistry, College of Chemistry, Jilin University, 
      Changchun 130021, PR China. Electronic address: zzq@jlu.edu.cn.
FAU - Feng, Guo-Dong
AU  - Feng GD
AD  - Department of Analytical Chemistry, College of Chemistry, Jilin University, 
      Changchun 130021, PR China. Electronic address: fenggd@jlu.edu.cn.
LA  - eng
PT  - Journal Article
DEP - 20170405
PL  - England
TA  - Food Chem
JT  - Food chemistry
JID - 7702639
RN  - 0 (Tetracyclines)
SB  - IM
MH  - Animals
MH  - Chromatography, High Pressure Liquid
MH  - Food Analysis
MH  - Food Contamination
MH  - Liquid Phase Microextraction
MH  - Liquid-Liquid Extraction
MH  - *Milk
MH  - *Tetracyclines
OTO - NOTNLM
OT  - Chlorotetracycline (PubChem CID: 54675777)
OT  - Doxycycline (PubChem CID: 54671203)
OT  - Dynamic liquid-liquid micro-extraction
OT  - Hollow fiber membrane
OT  - Ionic liquid
OT  - Milk
OT  - Oxytetracycline (PubChem CID: 54675779)
OT  - Tetracycline (PubChem CID: 54675776)
OT  - Tetracyclines
EDAT- 2017/05/12 06:00
MHDA- 2017/08/17 06:00
CRDT- 2017/05/12 06:00
PHST- 2016/04/27 00:00 [received]
PHST- 2016/08/11 00:00 [revised]
PHST- 2017/04/02 00:00 [accepted]
PHST- 2017/05/12 06:00 [entrez]
PHST- 2017/05/12 06:00 [pubmed]
PHST- 2017/08/17 06:00 [medline]
AID - S0308-8146(17)30565-4 [pii]
AID - 10.1016/j.foodchem.2017.04.021 [doi]
PST - ppublish
SO  - Food Chem. 2017 Oct 1;232:198-202. doi: 10.1016/j.foodchem.2017.04.021. Epub 2017 
      Apr 5.