PMID- 28833742 OWN - NLM STAT- MEDLINE DCOM- 20181015 LR - 20191210 IS - 1600-0668 (Electronic) IS - 0905-6947 (Linking) VI - 28 IP - 1 DP - 2018 Jan TI - Application of a novel reference material in an international round robin test on material emissions testing. PG - 181-187 LID - 10.1111/ina.12421 [doi] AB - Emission testing of products is currently a rapidly increasing field of measurement activity. Labeling procedures for construction products are based on such emission test chamber measurements, and hence, measurement performance should be verified. One possible route is to conduct testing of one material in different laboratories within a round robin test (RRT), ideally using homogeneous reference materials, which can be used within interlaboratory studies or as part of the quality management system to ensure comparable results. The applicability of a lacquer system with nine added VOCs (hexanal, styrene, n-decane, limonene, 2-ethyl-1-hexanol, N-methyl-alpha-pyrrolidone, 2-ethylhexyl acrylate, dimethyl phthalate, and n-hexadecane) was evaluated in an international RRT with 55 participating laboratories. An intralaboratory quality check confirmed the homogeneity and reproducibility of the lacquer material for most of the compounds (RSD 5%-6%), which was confirmed in the RRT. However, emissions varied for the polar compound N-methyl-alpha-pyrrolidone and the higher boiling compounds 1,2-dimethyl phthalate, and n-hexadecane which could be traced back to analytical issues. In the RRT, the interlaboratory relative standard deviations (RSDs) ranged from 30% to 65% for all participants but for reference laboratories the range was between 20% and 45%. CI - (c) 2017 The Authors. Indoor Air published by John Wiley & Sons Ltd. FAU - Horn, W AU - Horn W AUID- ORCID: 0000-0003-3926-4081 AD - Bundesanstalt fur Materialforschung und -prufung (BAM), Berlin, Germany. FAU - Richter, M AU - Richter M AUID- ORCID: 0000-0003-1402-249X AD - Bundesanstalt fur Materialforschung und -prufung (BAM), Berlin, Germany. FAU - Nohr, M AU - Nohr M AD - Markes International GmbH, Neu-Isenburg, Germany. FAU - Wilke, O AU - Wilke O AD - Bundesanstalt fur Materialforschung und -prufung (BAM), Berlin, Germany. FAU - Jann, O AU - Jann O AUID- ORCID: 0000-0002-4936-9605 AD - Bundesanstalt fur Materialforschung und -prufung (BAM), Berlin, Germany. LA - eng PT - Evaluation Study PT - Journal Article DEP - 20170911 PL - England TA - Indoor Air JT - Indoor air JID - 9423515 RN - 0 (Volatile Organic Compounds) SB - IM MH - Air/analysis MH - Construction Materials/*analysis MH - *Materials Testing MH - Reference Standards MH - Volatile Organic Compounds/analysis/*standards MH - Volatilization OTO - NOTNLM OT - QA/QC OT - VOC OT - emission test chamber OT - reference material OT - round robin test EDAT- 2017/08/24 06:00 MHDA- 2018/10/16 06:00 CRDT- 2017/08/24 06:00 PHST- 2017/03/16 00:00 [received] PHST- 2017/08/15 00:00 [accepted] PHST- 2017/08/24 06:00 [pubmed] PHST- 2018/10/16 06:00 [medline] PHST- 2017/08/24 06:00 [entrez] AID - 10.1111/ina.12421 [doi] PST - ppublish SO - Indoor Air. 2018 Jan;28(1):181-187. doi: 10.1111/ina.12421. Epub 2017 Sep 11.